Ti3SiC2/TiB2 composite was successfully obtained by hot pressing Ti/TiC/Si/B4C power mixtures.Volume fraction of TiB2 in Ti3SiC2/TiB2 composite can not exceed 10%.Incorporation of excessive TiB2 will affect the reactions process.TiC and Ti5Si3 were two important intermediate phases during the whole reactions.The microstructure characteristics of the Ti3SiC2/TiB2 composites were analyzed using scanning electron microscopy (SEM) and transmission electron microscopy (TEM).The experimental results show that the grains of Ti3SiC2/TiB2 composite are structured in a layered form,and the formation of TiB2 particles as reinforcements with elongated or equiaxed shape distributes in Ti3SiC2 matrix.
参考文献
[1] | Michel W.Barsoum .The M_(N+1)AX_N Phases: A new Class of solids; Thermodynamically Stable Nanolaminates[J].Progress in Solid State Chemistry,2000(1/4):201-281. |
[2] | Michel W. Barsoum;Tamer El-Raghy .The MAX Phases: Unique New Carbide and Nitride Materials[J].American Scientist,2001(4):334-343. |
[3] | S.-B. Li;J.-X. Xie;L.-T. Zhang .In situ synthesis of Ti_3SiC_2/SiC composite by displacement reaction of Si and TiC[J].Materials Science & Engineering, A. Structural Materials: Properties, Misrostructure and Processing,2004(1/2):51-56. |
[4] | R. Radhakrishnan;C. H. Henager Jr;J. L. Brimhall;S. B. Bhaduri .Synthesis of Ti3SiC2/SiC and TiSi2/SiC composites using displacement reactions in the Ti---Si---C system[J].Scripta materialia,1996(12):1809-1814. |
[5] | Y M Luo;S Li;J Chen;R Gang J Qiang W Pan .Fabrication Al2O3-Ti3SiC2 Composites and Mechanical Properties Evaluation[J].Materials Research Bulletin,2003,38:69-78. |
[6] | Wang HJ;Jin ZH;Miyamoto Y.Effect of Al2O3 on Mechanical Properties of Ti3SiC2/Al2O3 Composites[J].Ceramics International,2002(28):931-934. |
[7] | T El-Raghy;M W Barsoum;A Zavaliangos;S Kalidindi .Processing and Mechanical Properties of Ti3SiC2.Part Ⅱ:Effect of Grain Size and Deformation Temperature[J].Journal of the American Ceramic Society,1999,82:2855-2859. |
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