In order to investigate the effect of sintering temperature on aging properties and mechanical properties of 3Y-TZP dental ceramic in simulated oral environment,3Y-TZP nanopowder compacts were pressurelessly sintered at 1 350 ℃,1 400 ℃,1 450 ℃,1 500 ℃,respectively,then were treated by soaking in artificial saliva (65 ℃,pH=7) for two months.The treated specimens sintered at 1 350 ℃ showed there was no phase transformation but whose strength and toughnesswere significantly improved (P<0.05),while those sintered at 1 400 ℃-1 500 ℃ revealed a small amount of phase transformation and insignificant mechanical reinforcement (P>0.05).No micro-cracks were detected but increment in lattice volume was found in all specimens.Lowering sintering temperature favors aging resistance and mechanical reinforcement of 3Y-TZP in a simulated oral environment.
参考文献
[1] | Guo, Xin .On the degradation of zirconia ceramics during low-temperature annealing in water or water vapor[J].The journal of physics and chemistry of solids,1999(4):539-546. |
[2] | Papanagiotou HP;Morgano SM;Giordano RA;Pober R .In vitro evaluation of low-temperature aging effects and finishing procedures on the flexural strength and structural stability of Y-TZP dental ceramics.[J].The Journal of Prosthetic Dentistry,2006(3):154-164. |
[3] | Fukatsu K;Pezzotti G;Hayaishi Y;Sugano N .Evaluation of phase stability in zirconia femoral heads from different manufacturers after in vitro testing or in vivo retrieval.[J].The Journal of arthroplasty,2009(8):1225-1230. |
[4] | T. Kosmac;C. Oblak;P. Jevnikar .The effect of surface grinding and sandblasting on flexural strength and reliability of Y-TZP zirconia ceramic[J].Dental materials,1999(6):426-433. |
[5] | George A. Gogotsi .Fracture behaviour of Mg-PSZ ceramics: Comparative estimates[J].CERAMICS INTERNATIONAL,2009(7):2735-2740. |
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