建立了灰化处理-火焰原子吸收光谱测定载金炭中银量的方法；经过大量的条件实验，确定了坩埚材料、灰化温度、溶样试剂用量、测定介质酸度等最佳实验条件；在加入一定量单元素及混合元素的条件下，进行了银量测定的干扰实验。该方法操作简单快速、易于掌握，加入标准物质回收率为99．23％～102．5％，适合于批量载金炭样品的测定。
An ashing-FAAS(flame atomic absorption spectrometry ) determination method is used in determining silver content in gold-bearing carbon.Related parameters such as crucible materials,ashing temperature,dosage of dis-solving agents and acidity of media are determined through lots of experiments .With addition of certain amount of sin-gle element and mixed elements,interference experiment of silver determination is conducted .The method is easy to operate and to master,and recovery rate reaches 99.23 %to 102.5%with the addition of standard susbstance ,fitful for batch tests of gold-bearing carbon.
参考文献
| [1] | 陈港泉,黑文龙,毛振才.空气-乙炔火焰原子吸收法快速测定载金炭中金[J].分析测试技术与仪器,2000(01):42-44. |
| [2] | 唐文涛.载金炭中金的分析方法研究[J].宁夏工程技术,2003(03):243-245. |
| [3] | 夏珍珠.火焰原子吸收光谱法测定载金炭中金[J].黄金,2012(04):52-54. |
| [4] | 丁凤珍;黄福滨 .载金炭分析方法[J].地质实验室,1999,15(04):232-234. |
| [5] | 丘星初,丘山.氰化镀银溶液中银的光度测定[J].电镀与精饰,2000(05):39-41. |
| [6] | 刘茂荣.容量法测定方铅矿中高含量银[J].岩矿测试,2001(02):147-149. |
| [7] | 郑丽红;陈旭东;周红.石墨炉原子吸收光谱分析测定水中毒物银[J].仪器仪表与分析监测,2000(04):47-49. |
| [8] | GB/T 29509.2-2013.载金炭化学分析方法[S].北京:中国标准出版社,2013. |
- 下载量()
- 访问量()
- 您的评分：
-
10%
-
20%
-
30%
-
40%
-
50%