欢迎登录材料期刊网

材料期刊网

高级检索

以无水乙醇为隔离剂,通过湿法球磨制备了片型羰基铁粉,研究了球料比对片型化过程、电磁性能的影响。结果表明:增加球料比,羰基铁粉片型化更充分,晶粒尺寸减小;粒子的各向异性提高了片型羰基铁粉的微波电磁性能。以环氧树脂为基体树脂,填充体积分数30%的吸波剂制备了1.0mm 单层吸波涂层,在 X-Ku 波段反射率小于-7.5dB 的带宽大于10GHz,涂层最小面密度为2.96kg /m2。

The flake-shaped carbonyl iron powder(FCIP)was prepared by wet ball mill method with ethanol as isolation agent(0.1 nm).The influence of the ratio of ball to powder on the flake-shaped process and electromagnetic parameter was studied.The results show that the grain size of FCIP gradually is decreased and the anisotropy is increased significantly with the enhancing of the ratio of ball to powder.The dielectric loss and magnetic loss microwave performance are enhanced significantly attributed to the anisotropy of the FCIP.Epoxy resin is applied as bonders.The single-layer microwave absorbing coating with 1 .0 mm in thickness is prepared by u-sing epoxy resin as a matrix and the FCIP with the volume fraction of 30%.The lightest coating weights 2.96 kg /m2 ,when it meets the request of band width more than 10 GHz,and the reflectivity is less than -7.5 dB at the frequency range of 8-18 GHz.

参考文献

[1] 王永辉;赛义德;黄昊;薛方红;张黎;董星龙.铁纳米粒子/碳纤维/环氧树脂基复合材料的制备和吸波性能[J].材料研究学报,2015(2):81-87.
[2] 郭飞;杜红亮;屈绍波;夏颂;徐卓;赵建峰.海胆状氧化锌/羰基铁粉核壳结构复合粒子的抗氧化及吸波性能[J].无机化学学报,2015(4):755-760.
[3] 姜晓文;江振经;黄大庆.石油磺酸钡对微波吸收涂层的耐腐蚀性能的影响[J].航空材料学报,2015(2):72-76.
[4] 高海涛;王建江;娄鸿飞;蔡旭东;侯永伸.片状吸波剂的特点及其制备方法研究现状[J].材料导报,2014(11):69-73,93.
[5] Milica Vucinic-Vasic;Marko Boskovic;Aleksandar Antic.Temperature induced evolution of structure/microstructure parameters and their correlations with electric/magnetic properties of nanocrystalline Nickel ferrite[J].CERAMICS INTERNATIONAL,20143(3):4521-4527.
[6] Mahmoud Goodarz Naseri;M.K. Halimah;Arash Dehzangi;Ahmad Kamalianfar;Elias B. Saion;Burhanuddin Y. Majlis.A comprehensive overview on the structure and comparison of magnetic properties of nanocrystalline synthesized by a thermal treatment method[J].The journal of physics and chemistry of solids,20143(3):315-327.
[7] Wang, Wei;Guo, Jiaxiong;Long, Chang;Li, Wei;Guan, Jianguo.Flaky carbonyl iron particles with both small grain size and low internal strain for broadband microwave absorption[J].Journal of Alloys and Compounds: An Interdisciplinary Journal of Materials Science and Solid-state Chemistry and Physics,2015:106-111.
[8] Oliveira, F. A. C.;Marcelo, T.;Alves, C.;Santos, M.;Mascarenhas, J.;Trindade, B..Effect of particle size of starting oxide powders on the performance of doped-lanthanum oxyapatite produced by mechanical alloying followed by microwave sintering[J].Advanced Powder Technology: The internation Journal of the Society of Powder Technology, Japan,20145(5):1455-1461.
[9] Deng LJ;Zhou PH;Xie JL;Zhang L.Characterization and microwave resonance in nanocrystalline FeCoNi flake composite[J].Journal of Applied Physics,200710(10):3916-1-3916-6-0.
[10] Yin, C.;Fan, J.;Bai, L.;Ding, F.;Yuan, F..Microwave absorption and antioxidation properties of flaky carbonyl iron passivated with carbon dioxide[J].Journal of Magnetism and Magnetic Materials,2013:65-69.
[11] 赵立英;金平平;刘平安.非离子型水性环氧固化剂的制备与性能[J].高分子材料科学与工程,2014(9):20-23.
[12] 赵立英;曾凡聪;廖应峰;刘平安.球磨时间对片型羰基铁粉微波吸收剂结构和性能的影响[J].中南大学学报(自然科学版),2015(1):94-98.
[13] E.K. Cho;H.T. Kwon;E.M. Cho.The control of nano-grain size and magnetic properties of Fe_(73)Si_(16)B_7Nb_3Cu_1 soft magnetic powder cores[J].Materials Science & Engineering, A. Structural Materials: Properties, Misrostructure and Processing,20070(0):368-370.
[14] Sung-Soo Kim;Sun-Tae Kim;Yeo-Choon Yoon;Kyung-Sub Lee.Magnetic, dielectric, and microwave absorbing properties of iron particles dispersed in rubber matrix in gigahertz frequencies[J].Journal of Applied Physics,200510(10):10F905-1-10F905-3-0.
[15] 李晓光;吕华良;姬广斌;张豹山;唐东明.球磨钢珠配比对片状羰基铁粉吸波性能影响的研究[J].航空材料学报,2013(5):46-53.
上一张 下一张
上一张 下一张
计量
  • 下载量()
  • 访问量()
文章评分
  • 您的评分:
  • 1
    0%
  • 2
    0%
  • 3
    0%
  • 4
    0%
  • 5
    0%