{"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"以邻甲苯胺单体为原料、过硫酸铵为氧化剂,加入质量分数为0.0％、7.5％和14.9％的纳米TiO2,采用原位聚合法制备了聚邻甲苯胺均聚物以及聚邻甲苯胺/纳米TiO2复合物,利用扫描电镜、红外光谱、紫外-可见光谱和X射线衍射对其进行了结构表征.采用该复合物、聚邻甲苯胺和聚苯胺为填充物,以3％和5％的用量添加到环氧树脂(EP)/聚酰胺固化剂体系中,在碳钢表面制备了不同环氧涂层,测试了涂层的力学性能,发现上述填充物具有增强环氧涂层对腐蚀介质的阻隔的性能,其中含5％聚苯胺、5％聚邻甲苯胺、5％聚邻甲苯胺/TiO2(质量分数7.5％)复合物和3％聚邻甲苯胺/TiO2(质量分数14.9％)复合物的环氧涂层的力学性能较佳.通过极化曲线和交流阻抗谱对比研究了该4种环氧涂层在3.5％ NaCl溶液中的耐蚀性能.结果表明,含5％聚邻甲苯胺/TiO2(质量分数7.5％)复合物的环氧涂层具有最佳的耐蚀性.","authors":[{"authorName":"王勇","id":"8543e771-7132-48dd-ae8b-b4a27b458d81","originalAuthorName":"王勇"},{"authorName":"胡传波","id":"76614293-3c49-43e7-8e1a-fc1bf5c5a6c1","originalAuthorName":"胡传波"},{"authorName":"郑燕升","id":"8c431aa2-7906-461d-ab0c-30531a92f76d","originalAuthorName":"郑燕升"},{"authorName":"王发龙","id":"64dc380e-4f83-46f8-9056-44a58c90d363","originalAuthorName":"王发龙"},{"authorName":"莫春燕","id":"d9b78dcb-ec44-4f0f-8078-7fcf59fc40b4","originalAuthorName":"莫春燕"},{"authorName":"青勇权","id":"2963083b-b0ee-4aaf-b092-0438afa31927","originalAuthorName":"青勇权"},{"authorName":"莫倩","id":"1e1d3c7f-cd6b-4bcf-89ef-bf5cfe9befd9","originalAuthorName":"莫倩"}],"doi":"","fpage":"592","id":"0e4acf9f-87d5-4f13-8b91-f8e391bf722e","issue":"14","journal":{"abbrevTitle":"DDYTS","coverImgSrc":"journal/img/cover/DDYTS.jpg","id":"21","issnPpub":"1004-227X","publisherId":"DDYTS","title":"电镀与涂饰 "},"keywords":[{"id":"0bca038b-8c7b-47ec-8bbc-ac0a58ab1200","keyword":"聚邻甲苯胺","originalKeyword":"聚邻甲苯胺"},{"id":"4f687bd0-17c4-4ccf-a1eb-7721f57cd725","keyword":"纳米二氧化钛","originalKeyword":"纳米二氧化钛"},{"id":"bccd2acc-65b5-4d90-992b-c107474d4e1c","keyword":"原位聚合法","originalKeyword":"原位聚合法"},{"id":"621c6545-79f6-4168-af92-4ad39f27ab15","keyword":"环氧涂层","originalKeyword":"环氧涂层"},{"id":"52bba463-0ff5-481a-8c0b-0f7a5e0c2cde","keyword":"耐蚀性","originalKeyword":"耐蚀性"}],"language":"zh","publisherId":"ddyts201414002","title":"聚邻甲苯胺/纳米二氧化钛环氧复合涂层的性能","volume":"33","year":"2014"},{"abstractinfo":"通过十二氟庚基丙基三甲氧基硅烷对ZnO粒子进行改性，使ZnO表面由亲水性变为疏水性，然后将改性ZnO粒子与低表面能的热塑性树脂聚苯乙烯杂合，于160°C下烘烤25 min，在钢片上制得改性ZnO/聚苯乙烯复合超疏水涂层。采用红外光谱、扫描电镜和接触角分析仪对涂层表面结构和疏水性进行了研究。结果表明，改性后的 ZnO 粒子表面引入了疏水性的─CH3和─CF2─，形成微/纳米双重粗糙结构。当改性ZnO和聚苯乙烯的质量比为7∶3时，所得复合涂层表面与水的静态接触角为156°，滚动角8°，与钢片的附着力为2级，硬度B~H，冲击强度大于50 kg?cm，吸水率为7.3%，具有良好的应用前景。","authors":[{"authorName":"青勇权","id":"4e1ace82-f394-427b-9cce-960f4df621e0","originalAuthorName":"青勇权"},{"authorName":"郑燕升","id":"a9962d36-6f64-4e37-a870-9679afebbda1","originalAuthorName":"郑燕升"},{"authorName":"胡传波","id":"5d454714-8633-4568-953e-5fbb5b078522","originalAuthorName":"胡传波"},{"authorName":"王勇","id":"eb92e5c8-f951-4b08-a4b3-b08f9117f246","originalAuthorName":"王勇"},{"authorName":"龚勇","id":"a24ebe9c-d455-4b5a-b4c9-e78a216c3576","originalAuthorName":"龚勇"},{"authorName":"何易","id":"f74c8528-3959-4a20-bf86-19c78f09cb9c","originalAuthorName":"何易"},{"authorName":"莫倩","id":"4fe9d51d-9f1c-411d-8fd1-476131e46af4","originalAuthorName":"莫倩"}],"doi":"","fpage":"59","id":"2da7946c-9e69-4e4f-a9f4-ea9508a29d88","issue":"8","journal":{"abbrevTitle":"DDYTS","coverImgSrc":"journal/img/cover/DDYTS.jpg","id":"21","issnPpub":"1004-227X","publisherId":"DDYTS","title":"电镀与涂饰 "},"keywords":[{"id":"4f62b3f9-4465-44bd-9238-3b8e49f5a9b6","keyword":"超疏水涂层","originalKeyword":"超疏水涂层"},{"id":"dbc856e8-f34a-4ff3-ad72-695f37e1da9e","keyword":"氧化锌","originalKeyword":"氧化锌"},{"id":"cf0844a7-9574-4ea7-a8be-ef2c0c201e29","keyword":"十二氟庚基丙基三甲氧基硅烷","originalKeyword":"十二氟庚基丙基三甲氧基硅烷"},{"id":"60e61d2d-4c61-4bf7-91ab-45e160910446","keyword":"改性","originalKeyword":"改性"},{"id":"bbf098de-b994-438d-89fa-f45f6a2ec5e8","keyword":"聚苯乙烯","originalKeyword":"聚苯乙烯"},{"id":"3a9e9335-6bb8-4799-88cb-0e5a466755db","keyword":"疏水性","originalKeyword":"疏水性"}],"language":"zh","publisherId":"ddyts201308016","title":"氧化锌/聚苯乙烯超疏水复合涂层的制备及其性能","volume":"","year":"2013"},{"abstractinfo":"在纳米 SiC 存在的情况下，以苯胺单体为原料，过硫酸铵为氧化剂，采用化学氧化聚合法制备了聚苯胺/纳米 SiC 复合物。采用 SEM、XRD、UV-vis 等方法对产物进行形貌观察和结构表征。将涂层中分别含有聚苯胺和聚苯胺/纳米 SiC 复合物填料成的碳钢片浸泡于3．5％ NaCl 溶液中，通过开路电位、极化曲线和电化学阻抗谱来评价涂层的防腐蚀性能。结果表明，涂层中含有聚苯胺/纳米 SiC 复合物填料成分的碳钢片抗腐蚀能力强于含聚苯胺的碳钢片，腐蚀电位最高，腐蚀电流密度最小；而裸钢片腐蚀电位最小，腐蚀电流密度最大。","authors":[{"authorName":"胡传波","id":"fa91b5c3-88d5-42c4-a8b6-7a7eef7462aa","originalAuthorName":"胡传波"},{"authorName":"郑燕升","id":"337062d6-93e7-4d9b-82d9-3ffa40100aec","originalAuthorName":"郑燕升"},{"authorName":"莫春燕","id":"11b605bd-dbd3-4ca3-8e54-53826e911466","originalAuthorName":"莫春燕"},{"authorName":"王发龙","id":"3820f0ff-9e9b-4d5b-916b-020f14c3a404","originalAuthorName":"王发龙"},{"authorName":"青勇权","id":"f42732cb-9366-4971-a4a9-9a83b3544d32","originalAuthorName":"青勇权"},{"authorName":"王勇","id":"d5c6e434-53e6-4081-8c89-cd4b24a66c9b","originalAuthorName":"王勇"},{"authorName":"莫倩","id":"f99ff2fe-dbdf-43d7-bbc7-d4376cf66cd3","originalAuthorName":"莫倩"}],"doi":"","fpage":"1002","id":"6dace0a1-4232-4b3a-89b4-e7c40e6d45ae","issue":"10","journal":{"abbrevTitle":"FSYFH","coverImgSrc":"journal/img/cover/FSYFH.jpg","id":"25","issnPpub":"1005-748X","publisherId":"FSYFH","title":"腐蚀与防护"},"keywords":[{"id":"370a6e80-5cf5-411f-9570-c35825f2baa7","keyword":"聚苯胺/纳米 SiC 复合物","originalKeyword":"聚苯胺/纳米 SiC 复合物"},{"id":"ac77ca2b-fd90-4b80-bd4f-9aa539dc833d","keyword":"开路电位","originalKeyword":"开路电位"},{"id":"223d669e-0bb9-411f-a9d0-f4ba5fb02576","keyword":"极化曲线","originalKeyword":"极化曲线"},{"id":"01675c98-ac3b-47a4-911d-1982be6dac1c","keyword":"电化学阻抗","originalKeyword":"电化学阻抗"},{"id":"3ab9af6b-ef3e-4399-80a1-c407428a0365","keyword":"防腐蚀性能","originalKeyword":"防腐蚀性能"}],"language":"zh","publisherId":"fsyfh201410011","title":"聚苯胺／纳米碳化硅／环氧复合涂层的制备及其防腐蚀性能","volume":"","year":"2014"},{"abstractinfo":"以苯胺单体为原料、过硫酸铵为氧化剂，采用化学氧化法制备了本征态聚苯胺，将其与纳米CaCO3通过溶液共混法制备了聚苯胺/CaCO3复合物。采用扫描电镜(SEM)、X射线衍射(XRD)、紫外-可见光谱(UV-Vis)和红外光谱(IR)对聚苯胺/CaCO3复合物进行了形貌观察和结构表征。分别以聚苯胺、聚苯胺/CaCO3复合物为填料，加入到环氧树脂(EP)/聚酰胺固化剂体系中，在碳钢表面制备了EP/聚苯胺和EP/聚苯胺/CaCO3复合涂层，通过开路电位、极化曲线和交流阻抗谱等电化学方法对比研究了裸钢以及含 EP 涂层、EP/聚苯胺涂层、EP/聚苯胺/CaCO3复合涂层的碳钢试片在3.5% NaCl溶液中浸泡不同时间的腐蚀行为。结果表明，聚苯胺膜较好地包覆在CaCO3纳米粒子表面；CaCO3的加入增强了涂层的致密性，提高了聚苯胺分子对金属基体的粘附力。含有聚苯胺/纳米CaCO3复合物的环氧涂层具有最强的抗腐蚀能力，其次为环氧/聚苯胺涂层；两者相比，EP/聚苯胺/CaCO3复合涂层的腐蚀电位正移了59 mV，腐蚀电流密度降低了63%。","authors":[{"authorName":"胡传波","id":"0364b733-805e-49fe-bf0b-7595d5a4b6c4","originalAuthorName":"胡传波"},{"authorName":"郑燕升","id":"622fdc11-ece1-465c-9603-bd2c594ed5df","originalAuthorName":"郑燕升"},{"authorName":"王发龙","id":"00838720-b85b-46cb-b266-18ffc5ba3e88","originalAuthorName":"王发龙"},{"authorName":"莫春燕","id":"e95460a2-4535-4916-ade3-b0e4ce795f93","originalAuthorName":"莫春燕"},{"authorName":"青勇权","id":"64efca8b-c6c9-4483-bc43-97f75863f5fb","originalAuthorName":"青勇权"},{"authorName":"王勇","id":"8f2f772d-4855-4360-8fb4-3086199e5180","originalAuthorName":"王勇"},{"authorName":"莫倩","id":"e0768f2f-2004-4717-b238-f27de2d985e8","originalAuthorName":"莫倩"}],"doi":"","fpage":"407","id":"76ed66ce-9c9d-4c77-a8b3-db7521e62adf","issue":"10","journal":{"abbrevTitle":"DDYTS","coverImgSrc":"journal/img/cover/DDYTS.jpg","id":"21","issnPpub":"1004-227X","publisherId":"DDYTS","title":"电镀与涂饰 "},"keywords":[{"id":"116a39b6-c52f-450d-88f1-d427c56ffdc2","keyword":"环氧涂层","originalKeyword":"环氧涂层"},{"id":"3b5c7a75-3578-45ab-a856-f7a6ee4487b7","keyword":"聚苯胺","originalKeyword":"聚苯胺"},{"id":"bfbc124c-c25c-4627-b49b-6fab8761956e","keyword":"碳酸钙","originalKeyword":"碳酸钙"},{"id":"0a1f61c4-cd0b-4a2e-9933-50f5092bec6e","keyword":"纳米颗粒","originalKeyword":"纳米颗粒"},{"id":"04ed1c1f-d500-49ab-b762-96858a929754","keyword":"复合物","originalKeyword":"复合物"},{"id":"094a1094-1e0e-4adc-8d68-d9cf7673c7ca","keyword":"防腐","originalKeyword":"防腐"}],"language":"zh","publisherId":"ddyts201410001","title":"聚苯胺/纳米碳酸钙复合物的制备及其防腐性能","volume":"","year":"2014"},{"abstractinfo":"目的：研究苯胺均聚物/环氧复合涂层和苯胺共聚物/环氧复合涂层在3.5%(质量分数,后同) NaCl 溶液中的耐腐蚀性能。方法采用化学氧化聚合法制备苯胺均聚物和共聚物,用 SEM,XRD,UV-vis和 IR 对产物进行表征,并通过电化学测试分析复合涂层在3.5% NaCl 溶液中的防腐性能。结果苯胺均聚物/环氧复合涂层和苯胺共聚物/环氧复合涂层都能对碳钢起到不同程度的防腐蚀效果,相比之下,苯胺共聚物/环氧复合涂层的腐蚀电位最高,腐蚀电流密度最小。结论苯胺共聚物在碳钢表面产生了一层钝化膜,使得苯胺共聚物/环氧复合涂层具有较好的耐腐蚀性能。","authors":[{"authorName":"胡传波","id":"c85ad652-f533-4d96-9c49-2563c86736df","originalAuthorName":"胡传波"},{"authorName":"郑燕升","id":"2d864c25-4b74-45b3-af42-6b529e748def","originalAuthorName":"郑燕升"},{"authorName":"杨世椿","id":"709fba72-06a9-45fb-aad3-763316790369","originalAuthorName":"杨世椿"},{"authorName":"王发龙","id":"547974a2-fdd6-44cf-8556-8e27c3e86202","originalAuthorName":"王发龙"},{"authorName":"莫春燕","id":"e3c9df68-da3b-414e-a250-7848377a9fa5","originalAuthorName":"莫春燕"},{"authorName":"青勇权","id":"d63b4651-544c-45c7-8846-d7a94693cb31","originalAuthorName":"青勇权"},{"authorName":"莫倩","id":"d82c5fce-1e60-4373-b9d2-6f62727c8b0e","originalAuthorName":"莫倩"}],"doi":"","fpage":"158","id":"b37e6522-4520-449d-abbd-6bf38c4ee181","issue":"4","journal":{"abbrevTitle":"BMJS","coverImgSrc":"journal/img/cover/BMJS.jpg","id":"3","issnPpub":"1001-3660","publisherId":"BMJS","title":"表面技术 "},"keywords":[{"id":"723c3e93-d686-482f-880e-b68749d84a59","keyword":"化学氧化聚合法","originalKeyword":"化学氧化聚合法"},{"id":"8468223f-d797-4d37-bf5e-f36eaf61f75a","keyword":"苯胺均聚物","originalKeyword":"苯胺均聚物"},{"id":"1f44a284-2103-4a4e-88dc-bec5b0e4d7a2","keyword":"苯胺共聚物","originalKeyword":"苯胺共聚物"},{"id":"eeb9d083-4356-4b08-b7f0-f94c7afecb9f","keyword":"环氧涂层","originalKeyword":"环氧涂层"},{"id":"cf04a776-d1f4-42be-b085-b8f8362d3bb5","keyword":"耐腐蚀性能","originalKeyword":"耐腐蚀性能"},{"id":"d082580c-ba01-4798-b090-89b38b7da47e","keyword":"钝化膜","originalKeyword":"钝化膜"}],"language":"zh","publisherId":"bmjs201404031","title":"苯胺均聚物（共聚物）/环氧复合涂层的制备及其防腐性能研究","volume":"","year":"2014"},{"abstractinfo":"将纳米TiO2和微米ZnO机械搅拌,制备了纳米TiO2/ZnO复合粒子.通过硬脂酸对其改性,于200℃下烘烤15 min,在钢试片上得到纳米TiO2/ZnO复合超疏水涂层.采用扫描电镜、红外光谱和接触角分析仪对涂层表面的形貌和疏水性进行了表征.结果表明,复合粒子经硬脂酸表面改性后引入了疏水性的甲基,形成微/纳米双重粗糙结构.当硬脂酸含量为9％时,所得涂层表面与水的静态接触角为165.3,滚动角4°.该涂层具有优异的耐溶解性、耐温性及自清洁性.","authors":[{"authorName":"青勇权","id":"cdc37dec-9427-4e5b-8cd3-f5dc9802179f","originalAuthorName":"青勇权"},{"authorName":"郑燕升","id":"e56979e2-9655-4d74-82b4-542ddb2dddcf","originalAuthorName":"郑燕升"},{"authorName":"何易","id":"881eb0bc-9a09-40e4-830c-39e68195abb9","originalAuthorName":"何易"},{"authorName":"胡传波","id":"24c442bd-a340-4a5c-82cc-494117db925b","originalAuthorName":"胡传波"},{"authorName":"莫倩","id":"06c88b3c-a46e-49f6-bdd8-8fd715d26a01","originalAuthorName":"莫倩"}],"doi":"","fpage":"55","id":"1aaab0f3-b58e-4fcd-b418-4382c35961bb","issue":"4","journal":{"abbrevTitle":"DDYTS","coverImgSrc":"journal/img/cover/DDYTS.jpg","id":"21","issnPpub":"1004-227X","publisherId":"DDYTS","title":"电镀与涂饰 "},"keywords":[{"id":"f76c0154-7c0b-4f86-b649-c66fee0303a2","keyword":"超疏水涂层","originalKeyword":"超疏水涂层"},{"id":"8b1223b0-6245-4db2-9ea5-e6f12ba22c86","keyword":"纳米二氧化钛","originalKeyword":"纳米二氧化钛"},{"id":"9d8f029e-9cfe-417b-9798-529b8c017db6","keyword":"氧化锌","originalKeyword":"氧化锌"},{"id":"d4bb29db-186c-44d8-8639-01bb7211d925","keyword":"硬脂酸","originalKeyword":"硬脂酸"},{"id":"cef8d87f-d090-44b9-8bba-6eb0186d29cd","keyword":"表面改性","originalKeyword":"表面改性"},{"id":"1fa508b9-e487-4e52-9f3a-436f287e5685","keyword":"自清洁","originalKeyword":"自清洁"}],"language":"zh","publisherId":"ddyts201304014","title":"纳米二氧化钛/氧化锌超疏水涂层的制备及其性能","volume":"32","year":"2013"},{"abstractinfo":"以三氯化铁为氧化剂,对甲苯磺酸为掺杂剂,采用化学氧化聚合法制得均聚物聚吡咯(PPy)、聚N-甲基吡咯(PNMPy)和共聚物聚吡咯-聚N-甲基吡咯(PPy-PNMPy).通过扫描电镜、X射线衍射仪、紫外可见分光光度计、傅里叶变换红外光谱仪表征了3种聚合物的微观结构.采用电化学方法和腐蚀溶液浸泡法对比研究了裸钢片、PU(聚氨酯)涂层以及PU-PPy、PU-PNMPy和PU-PPy-PNMPy复合涂层的防腐性能.结果表明,共聚物PPy-PNMPy的致密性优于均聚物PPy和PNMPy. PU-PPy-PNMPy复合涂层的防腐性能和力学性能最优.","authors":[{"authorName":"王发龙","id":"0447b76e-b209-4427-9aa4-6aa57c705d13","originalAuthorName":"王发龙"},{"authorName":"郑燕升","id":"ba67680c-9048-42e5-af2e-d2440c4f76e8","originalAuthorName":"郑燕升"},{"authorName":"莫春燕","id":"b1c7e071-3deb-4c59-825a-cbfcb9145e0c","originalAuthorName":"莫春燕"},{"authorName":"胡传波","id":"06483828-36fc-40bb-bff1-ed629c8bf277","originalAuthorName":"胡传波"},{"authorName":"莫倩","id":"af5f85fe-e1a7-4f2c-8c8a-5cb57fa3b3b2","originalAuthorName":"莫倩"}],"doi":"","fpage":"770","id":"8ce699c9-f305-420d-b861-9b6bafc544d3","issue":"14","journal":{"abbrevTitle":"DDYTS","coverImgSrc":"journal/img/cover/DDYTS.jpg","id":"21","issnPpub":"1004-227X","publisherId":"DDYTS","title":"电镀与涂饰 "},"keywords":[{"id":"b7335eb8-ab75-4821-92ce-b5980f216569","keyword":"吡咯","originalKeyword":"吡咯"},{"id":"bad7c5d4-5fc6-4f42-9402-77c4c115390d","keyword":"N-甲基吡咯","originalKeyword":"N-甲基吡咯"},{"id":"5026b036-9188-4659-a6b6-33adae7025e7","keyword":"共聚物","originalKeyword":"共聚物"},{"id":"17e545cc-dd73-49bc-92ce-c5c564ebd026","keyword":"化学氧化聚合","originalKeyword":"化学氧化聚合"},{"id":"86c92bc5-aa6b-4894-ae60-1f342adc047e","keyword":"防腐","originalKeyword":"防腐"}],"language":"zh","publisherId":"ddyts201514002","title":"聚吡咯-聚N-甲基吡咯复合涂料的制备及防腐性能","volume":"34","year":"2015"},{"abstractinfo":"莫来石纤维是一种重要的陶瓷材料,被广泛用作高温隔热材料、金属基或陶瓷基复合材料的增强体等.本文主要综述了莫来石纤维的多种制备方法,特别是重点介绍了溶胶-凝胶法制备多晶莫来石纤维的研究现状.在溶胶-凝胶法制备莫来石纤维的过程中,原材料的选择、单相和双相溶胶的制备以及各种因素都会影响水解和浓缩过程,并决定莫来石纤维的最终性能.最后对制备莫来石纤维的发展方向进行了展望.","authors":[{"authorName":"乔健","id":"2b78e4f9-9653-4c3e-aeb0-6d9a5dc7de1b","originalAuthorName":"乔健"},{"authorName":"刘和义","id":"07e6c913-5070-422e-baf7-e5bce0b603c9","originalAuthorName":"刘和义"},{"authorName":"崔宏亮","id":"17030668-1565-4839-aa9a-de39a574cdd0","originalAuthorName":"崔宏亮"},{"authorName":"朱玉龙","id":"1ddc686b-0f3c-4599-82f6-7a4b84207880","originalAuthorName":"朱玉龙"}],"doi":"","fpage":"3230","id":"0b0f907a-b927-480c-a0fb-85bd6c0942c3","issue":"12","journal":{"abbrevTitle":"GSYTB","coverImgSrc":"journal/img/cover/GSYTB.jpg","id":"36","issnPpub":"1001-1625","publisherId":"GSYTB","title":"硅酸盐通报 "},"keywords":[{"id":"5f7f406f-c912-4287-a720-88a57f85c663","keyword":"莫来石纤维","originalKeyword":"莫来石纤维"},{"id":"821c0edf-2e38-440f-8d7e-28c2c8f32d3b","keyword":"制备工艺","originalKeyword":"制备工艺"},{"id":"1431989e-f011-4d7b-883c-2007e1a3f292","keyword":"溶胶-凝胶法","originalKeyword":"溶胶-凝胶法"},{"id":"438def9a-646b-4e0c-9e86-2642100f44a8","keyword":"影响因素","originalKeyword":"影响因素"},{"id":"d2d0c491-afc0-4d55-8424-838b39f0d898","keyword":"进展","originalKeyword":"进展"}],"language":"zh","publisherId":"gsytb201412030","title":"莫来石纤维制备方法综述","volume":"33","year":"2014"},{"abstractinfo":"将莫来石先驱体溶胶预先引入到硫酸铝水溶液中,干燥后经1200℃煅烧获得氧化铝-莫来石复合粉料.研究了该粉料与硅溶胶混合获得的混合粉的烧结行为,并与氧化铝、莫来石晶种和硅溶胶三相混合获得的混合粉的烧结行为进行了分析比较.其中,两种混合粉料均是以理论莫来石组分进行配比(Al2O3:SiO2=72:28),并且两种混合粉中莫来石晶种的质量分数均为5%.实验结果表明:前者在1450℃烧结20 min即实现完全莫来石化,其显微结构为晶须状莫来石;后者在1500℃烧结20 min实现完全莫来石化,其显微结构为针状莫来石.","authors":[{"authorName":"陈照峰","id":"bc6b8ee8-3afb-46c7-93f3-93f0e3206dc8","originalAuthorName":"陈照峰"},{"authorName":"张显","id":"bad8e3c7-d03b-4d0e-a657-acd46f0c1290","originalAuthorName":"张显"},{"authorName":"张立同","id":"4e39d94c-30a7-4c37-8964-628f31ef1ded","originalAuthorName":"张立同"},{"authorName":"成来飞","id":"cde4d20d-f917-4810-878e-ef43b09e69c0","originalAuthorName":"成来飞"}],"doi":"10.3969/j.issn.1001-1935.2001.03.003","fpage":"131","id":"0dc26c6e-4fea-454c-90ca-7ad0ed75bdee","issue":"3","journal":{"abbrevTitle":"NHCL","coverImgSrc":"journal/img/cover/NHCL.jpg","id":"55","issnPpub":"1001-1935","publisherId":"NHCL","title":"耐火材料 "},"keywords":[{"id":"d0cdb32f-e642-4ba0-a0a9-9420187c57d3","keyword":"莫来石先驱体溶胶","originalKeyword":"莫来石先驱体溶胶"},{"id":"dc48e975-ddc0-40d4-b086-3577f4e3ae9b","keyword":"氧化铝-莫来石复合粉","originalKeyword":"氧化铝-莫来石复合粉"},{"id":"4e008ff9-4867-401e-9132-c7e78b19b8ee","keyword":"硅溶胶","originalKeyword":"硅溶胶"},{"id":"32a18b8a-caca-4048-bd2d-0a70a0126084","keyword":"莫来石晶种","originalKeyword":"莫来石晶种"},{"id":"1aa5cf3f-51af-4cf2-a05a-a8961661aef2","keyword":"烧结行为","originalKeyword":"烧结行为"}],"language":"zh","publisherId":"nhcl200103003","title":"氧化铝-莫来石复合粉对莫来石烧结行为的影响","volume":"35","year":"2001"},{"abstractinfo":"以微米Al2O3和纳米SiO2为原料,添加成型添加剂PVB,制备出了多晶莫来石纤维.借助差热-失重分析(DSC-TGA)、X射线衍射(XRD)及扫描电镜(SEM)分别对纤维的固相反应、相组成及表面形貌等进行了研究.DSC-FGA表明,在600℃以下PVB被完全排出,在1200℃左右纳米SiO2发生从非晶质到鳞石英的晶形转变,XRD分析显示1400℃以下没有莫来石生成,1500℃生成少量莫来石,1500℃到1600℃时,莫来石大量生成,纤维完全莫来石化,并从动力学上说明了Al2O3和SiO2是一步反应生成莫来石.通过SEM观察,由于PVB的大量挥发,使制得的纤维表面粗糙,脆性增加.","authors":[{"authorName":"张亚彬","id":"63d4e810-d290-44a9-82b2-630ac6b953f0","originalAuthorName":"张亚彬"},{"authorName":"李瑞","id":"caa2234a-ebc1-4f02-8499-07061dc9abb5","originalAuthorName":"李瑞"},{"authorName":"高积强","id":"e0626eb8-105c-4a2d-9aab-282f94216437","originalAuthorName":"高积强"}],"doi":"","fpage":"721","id":"c545d853-8649-4f51-af24-084d1a97ec87","issue":"z1","journal":{"abbrevTitle":"XYJSCLYGC","coverImgSrc":"journal/img/cover/XYJSCLYGC.jpg","id":"69","issnPpub":"1002-185X","publisherId":"XYJSCLYGC","title":"稀有金属材料与工程"},"keywords":[{"id":"0cf7065d-d770-4288-a72b-f184c381e4fd","keyword":"莫来石","originalKeyword":"莫来石"},{"id":"1cb0ae8a-3c09-4035-9080-4fbfcf34dd81","keyword":"纤维","originalKeyword":"纤维"},{"id":"320b4f90-4a5f-4641-acfe-0d29eb0450a6","keyword":"工艺","originalKeyword":"工艺"}],"language":"zh","publisherId":"xyjsclygc2008z1189","title":"莫来石连续纤维制备工艺","volume":"37","year":"2008"}],"totalpage":81,"totalrecord":803}