针对H13钢中大尺寸析出相的存在形式及形成机制进行研究.研究发现,H13钢中大尺寸析出相包含3类——富钒的(V,Mo,Cr,Fe)C类、富Mo-Cr的(V,Mo,Cr,Fe)C类及硫化锰.富钒的(V,Mo,Cr,Fe)C类大尺寸析出相形状多呈现长条形,尺寸达数十微米,部分依附于硫化锰形核的析出相成类椭圆形;富Mo-Cr的(V,Mo,Cr,Fe)C析出相无规则形貌,钼、铬原子分数比相差不大,钒原子分数稍低.根据复合大尺寸析出相的结合形式,可以推测出大尺寸析出相的析出顺序.硫化物首先析出,富钒类(V,Mo,Cr,Fe)C相随后,富Mo-Cr类(V,Mo,Cr,Fe)C相则最后析出.结合大尺寸析出相的成分特征,Thermo-calc计算结果与试验结果一致.
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