本文对利用雾化法直接制备出Y、Ti过饱和固溶的粉体合金,经短时机械合金化和热等静压成型制备纳米结构9Cr-ODS钢技术进行了研究.采用扫描电镜和X射线衍射研究雾化合金粉与短时球磨后雾化合金粉的形貌特征与组织的演化.通过高分辨透射电镜和电子背散射衍射研究热固化成型后ODS钢的微观组织.测试了雾化粉和球磨8h合金粉热固化成型样品的应力-应变曲线.结果表明,用短时球磨雾化粉制备的ODS钢晶粒尺寸更加细小、形成高密度纳米尺寸的析出相.与常规方法制备的ODS钢相比,抗拉强度略高、塑性显著提高、球磨时间大幅缩短.
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