目的:研究硅片经雾化施液抛光技术加工后存在的位错缺陷。方法应用化学腐蚀法、光学方法分析硅片不同部位的位错腐蚀形貌、位错密度及其分布,通过单因素实验研究雾化参数对位错形貌和位错密度的影响规律。在相同的工艺参数下,和传统抛光进行对比实验。结果雾化抛光硅片的平均位错密度为1.2×104/cm2,边沿处的位错密度小于其他区域。在相同的工艺参数下,雾化施液CMP的抛光液消耗量约为传统CMP的1/10,但硅片的位错腐蚀形貌和位错密度明显好于传统抛光,且蚀坑分布均匀分散,没有出现位错排等严重缺陷。通过增大雾化器的出雾量能有效改善硅片表层的位错缺陷。结论相对于传统抛光,雾化施液抛光技术能更加高效地去除硅片的位错缺陷。
ABSTRACT:Objective To study the dislocation defect of silicon wafer which was polished by ultrasonic atomization chemical me-chanical polishing ( CMP) . Methods The chemical etching method and optics method were used to analyze the morphology, densi-ty, and distribution of the dislocation etch pits. Besides, the influence of atomization quantity on the morphology and density of dis-location was studied by single factor experiment. Then comparative experiments were conducted with traditional CMP under the same conditions. Results The average dislocation density of the polished silicon wafer was about 1. 2×104/cm2 and the dislocation density in edge area was lower than other areas. Besides, the dislocation morphology and dislocation density of silicon wafer pol-ished by ultrasonic atomization CMP were obviously better than those treated by traditional CMP under the same conditions while thepolishing liquid consumption was about one tenth of traditional CMP. The dislocation etch pits distributed evenly and there were no serious flaws such as dislocation piles and so on. In addition to that, the dislocation defect could be effectively improved by increas-ing the quantity of atomization. Conclusion Ultrasonic atomization CMP removed the dislocation defect of silicon wafer more effi-ciently than traditional CMP.
参考文献
[1] | 苏建修,康仁科,郭东明.超大规模集成电路制造中硅片化学机械抛光技术分析[J].半导体技术,2003(10):27-32. |
[2] | 詹阳,周国安.化学机械抛光过程优化研究[J].电子工业专用设备,2009(04):37-39. |
[3] | HORN M .Antireflection Layers and Planarization for Micro-lithography[J].SOLID STATE TECHNOLOGY,1991,34(11):57-62. |
[4] | RAHU J .Consumables for the Chemical Mechanical Polis-hing of Dielectrics and Conductors[J].MRS,1994,337:13-15. |
[5] | 翟靖,李庆忠.一种使用超声波精细雾化施液的SiO2抛光液[J].半导体技术,2012(04):263-266,311. |
[6] | Antonov RD.;Johnson AT. .Subband population in a single-wall carbon nanotube diode[J].Physical review letters,1999(16):3274-3276. |
[7] | 吕海涛,张维连,左燕,步云英.化学腐蚀法研究蓝宝石单晶中的位错缺陷[J].半导体技术,2004(04):48-51. |
[8] | 杨培志,邓佩珍,殷之文,田玉莲.Yb∶YAG晶体的生长缺陷及位错走向[J].人工晶体学报,2000(04):399-403. |
[9] | Lu CW.;Chen JC. .Numerical computation of sapphire crystal growth using heat exchanger method[J].Journal of Crystal Growth,2001(2/4):322-329. |
[10] | 王陈,李庆忠,朱仌,闫俊霞.雾化施液CMP工艺及材料去除机制研究[J].润滑与密封,2014(02):56-60. |
[11] | 朱仌,李庆忠,王陈,刘晓鹏,钱善华.雾化施液CMP工艺及实验设备[J].江南大学学报(自然科学版),2013(06):698-702. |
[12] | PEI Z J;BILLINGSLEY S R;MIURA S .Grinding Induced Subsurface Cracks in Silicon Wafers[J].International Jour-nal of Machine Tools & Manufacture,1999,39(05):1103. |
[13] | Z. Y. Jia;J. X. Su;Z. J. Jin;D. M. Guo;L. P. Li .Friction Characteristic of Wafer Surface in Chemical Mechanical Polishing[J].Key engineering materials,2005(291/292):389-394. |
[14] | 曾贵平,曹余惠,殷绍唐.掺质YAG晶体中的缺陷[J].人工晶体学报,1999(04):354-358. |
[15] | 闵乃本.晶体生长的物理基础[M].上海:上海科学技术出版社,1982 |
[16] | Yongwu Zhao;L. Chang;S. H. Kim .A mathematical model for chemical-mechanical polishing based on formation and removal of weakly bonded molecular species[J].Wear: an International Journal on the Science and Technology of Friction, Lubrication and Wear,2003(3/4):332-339. |
[17] | 黄卫星 .超声雾化试验研究[D].江苏大学,2007. |
- 下载量()
- 访问量()
- 您的评分:
-
10%
-
20%
-
30%
-
40%
-
50%