用机械化学及热压烧结方法成功制备了高致密Ni-20Fe/Al2O3纳米复合材料.通过X-ray、FE-SEM、力学性能、磁性能测试,结果表明,复合后材料断裂韧性从纯α-Al2O3相的4.7 MPa·m1/2提高到6.2 MPa·m1/2(19%(Ni-20Fe)/Al2O3),断裂方式有沿晶断裂和穿晶断裂两种.当Ni-20Fe合金的体积百分数达到19%时,复合材料的饱和磁化强度达33 emu/g,矫顽力为200 Oe,且在低于500℃的情况下,矫顽力基本不随温度而变,具有良好的磁热稳定性.
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