采用浆料法结合真空浸渗工艺,制备了二维(2D)石英纤维增强多孔Si3N4-SiO2基复合材料.采用X射线衍射技术就粘结剂种类和氮化硅的加入对材料析晶性能的影响进行了分析,采用扫描电镜对不同浸渗次数复合材料的截面和断口形貌进行了观察,并采用裂纹偏转因子对复合材料断裂模式进行了分析.结果表明,粘结剂中杂质Na+促进了石英析晶,而Si3N4对石英析晶影响不大.增加浸渗次数虽不能有效提高复合材料强度,但却使裂纹偏转因子变小,断裂模式由韧性断裂向脆性断裂转变,断口形貌由纤维成束拔出变为多级拔出.
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