通过均匀沉淀法,将NiO复合于玻璃微球表面.制备了纳米NiO/玻璃微球复合粒子.X射线衍射(XRD)、扫描电镜(SEM)结果表明,经过共沉积后,在玻璃微球表面生成一层具有面心结构的NiO层,晶粒尺寸大约为14 nm,这些纳米NiO粒子以丝状胶连的形式附着于玻璃微球表面形成镀层.能谱分析(EDS)结果显示,纳米NiO粒子在玻璃微球表面形成了分布均匀的镀层.傅立叶变换红外光谱仪(FT-IR)表明,所制得的纳米NiO/玻璃微球复合粒子在近红外和远红外波段都表现出良好的红外吸收特性.
参考文献
| [1] | 费逸伟,黄之杰,刘芳,李华强.聚合物微球--新型热红外涂料用填料性能研究[J].材料科学与工程学报,2003,21(2):270-273.Fei Yiwei,Huang Zhijie,Liu Fang,Li Huaqiang.Research for polymer's tiny particle----A new type ingredient used for thermal infrared coating[J].Journal of Materials Science & Engineering,2003,21(2):270-273. |
| [2] | 孙世安,费逸伟,王协旗,孙元宝,彭秀华.红外烟幕材料及其发展趋势[J].红外技术,2005,27(2):164-166.Sun Shi'an,Fei Yiwei,Wang Xieqi,Sun Yuanbao,Peng Xiuhua.IR smoke screen material and its developing[J].Infra-red Technology,2005,27(2):164-166. |
| [3] | 刘元俊,冯永强,贺传兰,邓建国,冀克俭,张银生,孙思修.玻璃微珠增强硬质聚氨酯泡沫塑料的压缩性能及热稳定性[J].复合材料学报,2006,23(2):65-70.LiuYuanjun,Feng Yongqiang,He Chuanlan,Deng Jianguo,Ji Kejian,Zhang Yinsheng,Sun Sixiu.Compressive properties and thermal stability of glass bead reinforced rigid polyure-thane foams[J].Acta Materiae Compositae Sinica,2006,23(2):65-70. |
| [4] | 陈震霖,朱鹏,王晓东,黄培.填料特件对聚酰亚胺复合材料摩擦学性能的影响[J].复合材料学报,2006,23(3):49-53.Chen Zhenlin,Zhu Peng,Wang Xiaodong,Huang Pei.Effects of properties of the fillers on the polyimide composite tribologi-cal behaviors[J].Acta Materiae Compositae Siniea,2006,23(3):49-53. |
| [5] | Geleil A S,Hall M M,Shelby J E.Hollow glass microspheres for use in radiation shielding[J].Journal of Non-Crystalline Solids,2006,352(6/7):620-625. |
| [6] | Kim Jae-Han,Choi Won-Choon,Kim Hee-Young,Kang Yong,Park Yong-Ki.Preparation of mono-dispersed mixed metal oxide micro hollow spheres by homogeneous precipita-tion in a micro precipitator[J].Powder Technology,2005,153(1):166-175. |
| [7] | Geleil A S.Doped low Tg glasses as phosphor materials[J].Physics and Chemistry of Glasses,2005,46(4):404-411. |
| [8] | Shukla S,Seal S,Rahaman Z,Scammon K.Electroless copper coating of cenospheres using silver nitrate activator[J].Mate-rials Letters,2002,57(1):151-156 |
| [9] | 毛倩瑾,于彩霞,葛凯勇,周美玲.粉煤灰空心微珠的改性及其吸波特性[J].清华大学学报:自然科学版,2005,45(12):1672-1675.Mao Qianjin,Yu Caixia,Ge Kaiyong,Zhou Meiling.Micro-wave absorption characteristics of surface treated fly-ash ceno-sphere particles[J].J Tsinghua Univ:Sci & Tech,2005,45(12):1672-1675. |
| [10] | 刘家琴,吴玉程,薛茹君.空心微珠表面化学镀Ni-Co-P合金[J].物理化学学报,2006,22(2):239-243.Liu,Jiaqin,Wu Yucheng,Xue Rujun.Electroless plating Ni-Co-P alloy on the surface of fly ash cenospheres[J].Acta Phys Chim Sin,2006,22(2):239-243. |
| [11] | 杜军,史广旭,陶长元,汪宁,邱华.玻璃微球的表面化学镀银及红外辐射性能研究[J].压电与声光,2006,28(1):96-98.Du Jun,Shi Guangxu,Tao Changyuan,Wang Ning,Qiu Hua.Electroless silver planting and infrared radiation performance of hollow microsphere glass[J].Piezoelectrics & Acoustooptics,2006,28(1):96-98. |
| [12] | Cordente N,Toustou B,Colliere V,et al.New procedure to-wards well-dispersed nickel oxide nanoparticles of controlled size[J].Chimie/Chemistry,2001,4(2):143-148. |
| [13] | Akiba S,Hara W,Watanaba T,et al.Surface modification of silicate glasses by nanoimprint using nanostriped NiO thin film molds[J].Appl Surf Sci,2007,253(10):4512-4514. |
| [14] | Takahashi R,Sato S,Sodesawa T,et al.Ni/SiO2 prepared by sol-gel process using citric acid[J].Micro Meso Matl,2003,66(2):197-208. |
| [15] | Patil P S,Kadam L D.Preparation and characterization of spray pyrolyzed nickel oxide (NiO) thin films[J].Appl Surf Sci,2002,199(1/4):211-221. |
| [16] | Cerc Korosec R,Bukovec P,Pihlar B.Preparation and struc-tural investigations of electro -chromic nano-sized NiOx films made via the sol-gel route[J].Solid State Ionics,2003,165(1/4):191-200. |
| [17] | Wei Jing,Liu Jianhua,Li Songmei.Electromagnetic and mi-crowave absorption properties of Fe3O4 magnetic films plated on hollow glass spheres[J].Journal of Magnetism and Mag-netic Materials,2007,312(2):414-417. |
| [18] | Liu Jianhua,Wei Jing,Li Songmei.Preparation and character-istics of Fe3O4 magnetic thin films plated on hollow glass spheres[J].Materials Letters,2007,61(7):1529-1532. |
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