制备型液相色谱动态轴向压缩柱技术和应用

色谱 , 2004, 22(4): 403-407. doi: 10.3321/j.issn:1000-8713.2004.04.028

制备型液相色谱动态轴向压缩柱技术和应用

韩金玉 ^1, , 魏文英 ^2, , 常贺英 ^3, , 王华 ^4,

1.天津大学化工学院,绿色合成与转化教育部重点实验室,天津,300072

2.天津大学化工学院,绿色合成与转化教育部重点实验室,天津,300072

3.天津大学化工学院,绿色合成与转化教育部重点实验室,天津,300072

4.天津大学化工学院,绿色合成与转化教育部重点实验室,天津,300072

关键词：制备液相色谱 , 动态轴向压缩 , 柱装填

Technique and Application for Packing Preparative Liquid Chromatographic Column by Dynamic Axial Compression

综述了动态轴向压缩技术装填液相色谱柱的原理、装置及装置设计的发展状况,对动态轴向压缩装填过程和柱性能的影响因素如柱长、填料和调浆溶剂的性质、压缩压力进行了分析,讨论了柱内密度分布不均、柱壁效应两种现象和解决的办法,评价了这种技术的优缺点,介绍了其应用、发展现状与前景.引用文献50篇.

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制备型液相色谱动态轴向压缩柱技术和应用

Technique and Application for Packing Preparative Liquid Chromatographic Column by Dynamic Axial Compression

参考文献