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在阐述固相微萃取的平衡理论及非平衡理论基础上,重点探讨了萃取头的制备技术和相关试验方法的进展.除了介绍商品化通用萃取头的制备技术外,还论述了溶胶-凝胶法、电沉积法、碳素基体吸附法、高温环氧树脂固定法等新的制备技术;探讨了固相微萃取试验方法中萃取模式和萃取头的选择、萃取条件优化以及方法的灵敏度、精度、自动化等的评价;进一步总结了固相微萃取的应用现状,对固相微萃取的发展方向作了展望.

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