以激光为热源,以SiC纳米颗粒材料为前驱体,用激光照射SiC纳米颗粒原位生长晶须.结果表明:由于激光能量输出的瞬时特性,SiC纳米颗粒受到激光的照射可瞬时生成SiC晶须.随着激光功率的提高,晶须的直径从纳米级增大到微米级.由于在激光光斑内能量呈高斯分布,光斑内不同区域的SiC颗粒的温度不同,致使生成的晶须形态在不同的区域分别呈现为团絮状、网状和棒状等.X射线衍射分析表明,激光照射SiC纳米颗粒原位生长的晶须具有很高的纯度.
参考文献
[1] | Sumio Iijima,Helical microtubulee of graphitic carbon,Nature,354,56(1991) |
[2] | LI Wu,Inorganic Whisker (Beijing,Chemical Industry Press,2005) p.(李武,无机晶须(北京,化学工业出版社,2005)P. |
[3] | Shin ichi Honda,Yang Gyu Baeka,Takashi Ikuno,Hidekazu Kohara,Mitsuhiro Katayama,Kenjiro Oura,Takashi Hirao,SiC nanofibers grown by high power mi-crowave plasma chemical vapor deposition,Applied Sur-face Science,212-213(spec),378(2003) |
[4] | Deng S.Z.,Wu Z.S.,Jun Zhou,Xu N.S.,Jian Chen,Jun Chen,Synthesis of silicon carbide nano-junctions in a catalyst-assisted process,Chemical Physics Letters,364(5-6),608(2002) |
[5] | Meng G.W.,Zhang L.D.,Qin Y.,Mo C.M.,Phillipp F.,Synthesis of β-SiC nanowires with SiO2 wrappers,Nano Structured Materials,12(5-8),1003(1999) |
[6] | Ahn,Hyung Suk,Choi,Doo Jin,Fabrication of silicon car-bide whiskers and whisker-containing composite coatings without using a metallic catalyst,Surface and Coatings Technology,154(2-3),276(2002) |
[7] | Munoz E.,Dalton A.B.,Collins S.,Zakhidov A.A.,Baugh-man R.H.,Zhou W.L.,He,J.,O'Connor C.J.,McCarthy B.,Blau W.J.,Synthesis of SiC nanorods from sheets of single-walled carbon nanotubes,Chemical Physics Let-ters,359(5-6),397(2002) |
[8] | Botti S.,Ciardi R.,Asilyan L.,De Dominicis L.,Fabbri F.,Orlanducci S.,Fiori A.,Carbon nanotubes grown by laser-annealing of SiC nano-particles,Chemical Physics Letters,400(1-3),264(2004) |
[9] | CAO Xiaoming,ZHANG Jinsong,HU Wanping,DU Qingyang,The growth of SiC whiskers by in-situ on the surface of SiC foam ceramics,Chinese J.Material Re-search,20(3),291(2006)(曹小明,张劲松,胡宛平,杜庆洋,泡沫碳化硅陶瓷表面原位生长碳化硅晶须,材料研究学报,20(3),291(2006)) |
[10] | BAI Shuo,CHENG Huiming,SU Ge,WEI Yongliang,SHEN Zuhong,ZHOU Benlian,Growth mechanisim of dumbbell-shaped biomimetic SiC whiskers,Chinese J.Material Research,16(2),136(2002)(白朔,成会明,苏革,魏永良,沈祖洪,周本濂,哑铃形碳化硅晶须生长的机理,材料研究学报,10(2),136(2002)) |
上一张
下一张
上一张
下一张
计量
- 下载量()
- 访问量()
文章评分
- 您的评分:
-
10%
-
20%
-
30%
-
40%
-
50%