采用电弧离子镀技术在镍基单晶高温合金基体上制备了NiCoCrAlYSiB涂层和(NiCoCrAlYSiB+AlSiY)梯度涂层,对比研究了2种涂层退火态的组织结构和在1000,1100和1150℃下的恒温氧化行为.结果表明:退火处理后,NiCoCrAlYSiB涂层是由γ'/γ相和弥散其中的点状β-NiAl相构成;(NiCoCrAlYSiB+AlSiY)梯度涂层分为两层,外层以β-NiAl相为主,含有少量的Cr3Si相,内层和NiCoCrAlYSiB涂层的结构相似.NiCoCrAlYSiB涂层在1000℃下有良好的抗氧化性能,在1100和1150℃下因表面生成保护性较差的尖晶石相而快速退化;(NiCoCrAlYSiB+AlSiY)梯度涂层在1000-1150℃下均表现出良好的抗高温氧化性能,1100℃度下氧化300 h后仍有大量的β-NiAl相存在,1150℃下氧化300 h后涂层中Al含量仍在8%(质量分数)以上,少量的β-NiAl相和过饱和的,γ'/γ相可维持表面Al2O3膜的形成和修复.
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