采用超声辅助电镀法在Q235钢基体表面上制备了纳米叠层Ni镀膜.利用X射线衍射分析测定了镀膜的相结构和晶粒尺寸,在扫描电镜下观察了镀膜试样的剖面微观形貌,通过在室温7%HCl溶液中的浸泡实验考察了镀膜试样的耐腐蚀性能,采取磨轮磨损实验法对镀膜的耐磨性能进行了评价.结果显示,纳米叠层Ni镀膜沿着最密排的(111)晶面择优取向生长,其微结构明显呈平整层状重复堆积结构,普通电镀Ni镀膜的柱状晶垂直外延生长现象已被彻底消除.与普通电镀Ni镀膜相比,纳米叠层Ni镀膜的耐磨性能不仅明显改善,而且其耐腐蚀性能得到显著提高.
参考文献
[1] | Chen Y.Practical Electrodeposition Technology.Beijing:National Defence Industrial Press,2003:147(陈亚.现代实用电镀技术.北京:国防工业出版社,2003:147) |
[2] | Iwasaki H,Higashi K,Nieh T G.Scr Mater,2004; 50:395 |
[3] | Chen L,Wang L P,Zeng Z X,Zhang J Y.Mater Sci Eng,2006; A434:319 |
[4] | Hamid Z A,Ghayad I M.Mater Left,2002; 53:238 |
[5] | Erb U.Nanostruct Mater,1995; 6:533 |
[6] | Aruna S T,William G V K,Rajam K S.J Alloys Compd,2009; 468:546 |
[7] | He Y L.Electroplating Finish,2002; 21(2):1(何跃林.电镀与涂饰,2002; 21(2):1) |
[8] | Cheung C,Djuanda F,Erb U,Palumbo G.Nanostruct Mater,1995; 5:513 |
[9] | Cheng D,Yan Z J,Yan L.Acta Metall Sin,2008; 44:1461(程东,严志军,严立.金属学报,2008; 44:1461) |
[10] | Tayyebi M,Eghbali B.Mater Sci Eng,2013; A559:759 |
[11] | Menezes S,Anderson D P W.J Electrochem Soc,1990; 137:440 |
[12] | Rao S I,Hazzledine P M.Philos Mag,2000; 80A:2011 |
[13] | Rajasekaran N,Mohan S.Corros Sci,2009; 51:2139 |
[14] | Haseeb A S M A,Celis J P,Roos J R.J Electrochem Soc,1994; 141:230 |
[15] | Troyon M,Wang L.Appl Surf Sci,1996; 103:517 |
[16] | Wang Y,Deng Y Z,Ma Y T,Gao F.Surf Coat Technol,2011; 206:1203 |
[17] | Xie T T,Mao S D,Yu C,Wang S J,Song Z L.Vacuum,2012; 86:1583 |
[18] | Xia F F,Wu M H,Wang F,Jia Z Y,Wang A L.Curr Appl Phys,2009; 9(1):44 |
[19] | Zhu Y K,Yu Z M,Niu Y S,Ding W J.J Adhesion Sci Technol,2012; 26:1645 |
[20] | Xia F F,Liu C,Wang F,Wu M H,Wang J D,Fu H L,Wang J X.J Alloys Compd,2010; 490:431 |
[21] | Jensen J A D,Pocwiardowski P,Persson P O (A),Hultman L,M(o)ller P.Chem Phys Lett,2003; 368:732 |
[22] | Lorimer J P,Pollet B,Phull S S,Mason T J,Walton D J,Geissler U.Electrochim Acta,1996; 41:2737 |
[23] | Liu P S,Liang K M.J Mater Sci,2001; 36:5059 |
[24] | Chiu L H,Wu C H,Chang H.Corrosion,2007; 63:127 |
[25] | Mishra R,Balasubramaniam R.Corros Sci,2004; 46:3019 |
[26] | Cai J P,Lyon S B.Corros Sci,2005; 47:2956 |
上一张
下一张
上一张
下一张
计量
- 下载量()
- 访问量()
文章评分
- 您的评分:
-
10%
-
20%
-
30%
-
40%
-
50%