以商业活性炭为原料,采用真空浸渍法结合高温真空热处理工艺,制备出多孔C/Fe纳米复合材料.实验采用氮气吸附法测量了C/Fe纳米复合材料的比表面积和孔径分布,并利用XRD和TEM表征了其结构和形貌.实验结果显示:C/Fe纳米复合材料的比表面积为450～650m2/g,并保留了活性炭介孔尺度的多孔结构特性.C/Fe纳米复合材料由非晶碳、碳纳米带以及铁纳米粒子构成,纳米铁颗粒均匀分布在非晶碳基体中,石墨化的碳纳米带包裹纳米铁颗粒并向外伸展相互连接,形成碳纳米网络结构.并就反应过程以及过渡金属对非晶碳石墨化的催化机理进行了探讨.
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