铌的分析测定对于航天、电子、通讯、能源等行业的发展都具有重大意义.近年来各种新试剂、新方法的不断涌现,使铌的光度分析有了新的进展.通过对铌的光度分析试剂予以综述,重点介绍了各类显色剂及其显色反应体系、相应光度分析方法的最大吸收波长、摩尔吸光系数、检测限、干扰情况及其应用.
参考文献
| [1] | 何季麟.钽铌工业的进步与展望[J].稀有金属,2003(01):23-27. |
| [2] | 《岩石矿物分析》编写组.岩石矿物分析[M].北京:地质出版社,1991 |
| [3] | 北京矿冶研究总院测试研究所.有色冶金分析手册[M].北京:冶金工业出版社,2004 |
| [4] | Brykina G D;Lebedeva G G;Shpigun O A .Determination of niobium (V) with sulfochlorophenol S in mineral raw material by solid-phase spectrophotometry[J].Zavod Lab,1993,59(01):4. |
| [5] | 赵泓;潘教麦;余方多 等.间乙酰基氯磺酚光度法测定钢中的铌[J].化学试剂,1990,12(03):170. |
| [6] | 张钦;叶叙林 .铌(Ⅴ)与4,8-萘二磺酸偶氮氯磺酚显色反应的研究[J].冶金分析,1991,11(05):26. |
| [7] | 黄亚励,张华山,黎心懿.新显色剂6,8-二磺酸萘偶氮氯磺酚与铌（V）显色反应的研究及应用[J].分析试验室,1991(06):12. |
| [8] | 黄美新,林发.硝基磺酚S分光光度法测定硝酸溶液中微量铌[J].湘潭矿业学院学报,1993(03):69-73. |
| [9] | 程思传,潘教麦,徐仲隽.新显色剂间羧基偶氮苦胺酸光度法测定铌的研究--钢铁中微量铌的测定[J].分析试验室,1993(02):40. |
| [10] | 李先春;汤园平 .苦胺酸偶氮氯膦的合成及其与Nb(V)的显色反应[J].江西师范大学学报(自然科学版),1991,15(01):45. |
| [11] | 陶慧林.铌-偶氮胂Ⅲ-锌-邻二氮菲多元络合物显色反应的研究[J].分析试验室,2003(05):22-24. |
| [12] | 陶慧林.偶氮氯膦Ⅲ与铌的显色反应及其应用[J].桂林工学院学报,1999(02):169-172. |
| [13] | 陶慧林,纪向东,高春玲.偶氮氯膦-mA光度法测定铌[J].岩矿测试,2002(03):183-186. |
| [14] | 曾云鹗;张华山;陈震华.现代化学试剂手册 (第四分册) 无机离子显色剂[M].北京:化学工业出版社,1989 |
| [15] | 盘向军,姜南杰,朱理哲.2-[（5-溴-2-吡啶）-偶氮]-5-二乙氨基苯酚分光光度法测定岩石中微量铌[J].光谱实验室,2001(04):456-458. |
| [16] | 晋勇 .多元络合物在钽铌分析中的应用[J].稀有金属,1989,13(03):273. |
| [17] | Yu. M. Dedkov;N. V. Korsakova;O. G. Radugina .Color Reactions of Niobium and Tantalum with Bromine-Substituted Reagents of the PAR-PAN Group[J].Journal of analytical chemistry,2003(9):836-840. |
| [18] | 徐汾兰,徐炎.3,5-Br2-PADAP分光光度计测定钢铁中微量铌[J].华东冶金学院学报,1998(04):332-335. |
| [19] | 张华山;王红;仇佩虹 等.新显色剂 2-(5-硝基-2-吡啶偶氮)-5-二乙氨基苯酚与铌配合物的分光光度法研究[J].化学试剂,1995,17(01):1. |
| [20] | Anton R I;Marini H J;Olsina R A .Spectral studies of niobium complexes with 2-(5-chloro-2-pyridylazo)-5-dimethylaminophenol (5.ClDMPAP).Analytical applications[J].Analytical Letters,1995,28(04):663. |
| [21] | Alaa S.Amin .The surfactant-sensitized analytical reaction of niobium with some thiazolylazo compounds[J].Microchemical Journal: Devoted to the Application of Microtechniques in all Branches of Science,2000(3):261-267. |
| [22] | A И 拉扎列夫;孙淑嫒;孙龄高.金属分析中的有机试剂[M].北京:北京师范大学出版社,1983 |
| [23] | 陈必友;李启华.工厂分析化学手册[M].北京:化学工业出版社,2002:94. |
| [24] | Nagiev Kh D;Kulieva F V;Rustamova U M.Spectrophotometric study of the complex niobium(V) with 2,3,4-trioxy-phenylazo-5′-sulfonaphtalene in presence of CTMABr[J].Kimya Problemlari Jurnali,2003(03):40. |
| [25] | Dedkov Yu M .Structure of metal complexes of O,O′-dihydroxyphenylazonaphthyls and quantitative characteristics of the corresponding color reactions[J].JOURNAL OF ANALYTICAL CHEMISTRY,1995,50(11):1035. |
| [26] | Sanchez M J;Francisco A;Jimenez F et al.Complexation equilibria between niobium(V) and 4-(4′H-1′,2′,4′-triazolyl-3′-azo)-2-methylresorcinol[J].TALANTA,1989,36(08):831. |
| [27] | 罗宗铭;王秀云;周毅红 .在氨羧配合剂和阳离子表面活性剂存在下铌与二溴苯基荧光酮的显色反应及其应用[J].分析化学,1990,18(07):672. |
| [28] | 沈含熙;王连生.铌-酒石酸-邻硝基苯基荧光酮-CTMAB多元络合物显色反应的研究[J].化学通报(印刷版),1984(02):26. |
| [29] | 平锡康 .混合表面活性剂多元络合物光度法测定岩石中痕量铌[J].理化检验-化学分册,1992,28(03):18. |
| [30] | 陶慧林,钟福新.铌与溴邻苯三酚红和二安替比林甲烷多元络合物测定铌[J].桂林工学院学报,2003(04):473-476. |
| [31] | 李宽亮.理化分析测试指南金属材料部分钢铁化学分析手册[M].北京:国防工业出版社,1985:194. |
| [32] | 郭光熙 .胶束增溶分光光度法测定矿石中微量铌和钽[J].分析化学,1990,18(06):541. |
| [33] | 陶慧林;司得勇 .铌-铬天青S-氯代十六烷基吡啶体系光度法测定铌[J].桂林工学院学报,1998,18(02):179. |
| [34] | 李慧之;范荣;裴梅山 .微乳液介质-二甲氧基羟基苯基荧光酮催化光度法测定合金中铌[J].分析化学,2005,33(10):1513. |
| [35] | 王加林;李祖碧;徐其亨.罗丹明B-铌钼酸体系光度测定铌[J].云南化工,1993(01):34. |
| [36] | 陶慧林.铌-硫氰酸盐-丁基罗丹明B体系光度法测定铌[J].广西科学,2005(01):52-54. |
| [37] | 陶慧林 .聚乙烯醇和阿拉伯胶存在下用分光光度法测定铌[J].桂林工学院学报,1995,15(04):392. |
| [38] | 李祖碧;徐其亨 .铌(V)-硫氰酸盐-结晶紫高灵敏显色反应的研究及应用[J].稀有金属,1988,12(02):152. |
| [39] | 李祖碧;徐其亨 .耐尔蓝-铌钼杂多酸-聚乙烯醇-124体系测定铌[J].分析化学,1992,20(05):520. |
| [40] | Gromova T A;Elinson S V;Astafurov V I .Conditions for simultaneous photometric determination of zirconium and niobium in multicomponent alloys[J].Zavod Lab,1992,58(08):9. |
| [41] | Stoyanova I V;Vinarovs L I;Antonovich V P et al.Selective extraction-photometric method for determination of niobium in natural and technical materials[J].Zavod Lab,1992,58(08):13. |
| [42] | Chhakkar A K;Kakkar L R .Extractive spectrophotometric determinationof niobium(v) with 3-hydroxy-2-(2-thienyl)-4H-chromen-4-one[J].FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY,1995,351(08):720. |
| [43] | Nashine N;Mishra R K .Extraction-spectrophotometric determination of niobium with thiocyanate and N-hydroxy-N,N′-diphenylbenzamidine[J].Journal of the Indian Chemical Society,1993,70(07):661. |
| [44] | Mori I;Fujita Y;Toyoda M et al.Alternative spectrophotometric determination of niobium and tantalum with o-hydroxyhydroquinonephthalein in cationic surfactant micellar media.Application of xanthene derivatives in analyticalchemistry.Part XC[J].FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY,1992,342(1-2):80. |
| [45] | Muralikrishna U;Murty J A .Spectrophotometric determination of niobium through heteropoly blue formation[J].Journal of the Indian Chemical Society,1991,68(10):586. |
| [46] | Tarasiewicz M;Misiuk W;Tarasiewicz H P .Extractive spectrophotometric determination of niobium(V) with promazine hydrochloride[J].MICROCHEMICAL JOURNAL,1988,37:36. |
| [47] | N.Agnihotri;J.R.Mehta .A highly selective spectrophotometric determination of niobium(V) using 6-chloro-2-(2'-furyl)-3-hydroxy-4-oxo-4H-1-benzopyran as a complexing agent and chloroform as an extractant[J].Journal of the Indian Chemical Society,2003(9):837-840. |
| [48] | Inoue S;Mishima O;Zhang Q B et al.Spectrophotometric determination of niobium(V) with N-cinnamoyl-N-2,3-xylylhydroxylamine and thiocyanate[J].ANALYTICAL LETTERS,2002,34(14):2465. |
| [49] | Chhakkar A K;Kakkar L R .Extractive spectrophotometric determinationof niobium(V) using 3-hydroxyflavone[J].Microchimica Acta,1995,117(3-4):137. |
| [50] | Burns D T;Chimpalee D .Spectrophotometric determination of niobium after extraction with thiocyanate and 1-naphthylmethyltriphenylphosphonium chloride into microcrystalline 1,4-dichlorobenzene[J].Analytical Chemistry Acta,1992,256(02):307. |
| [51] | 张培善,杨主明,陶克捷,宋仁奎.我国铌钽稀土矿物学及工业利用[J].稀有金属,2005(02):206-210. |
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