以Ni-Al-Fe系合金中B2型金属间化合物NiAl(Fe)和α-Fe(Ni,Al)固溶体互为基体和析出相,主要研究了时效处理对其强度的影响及其时效组织特征.结果表明,以NiAl(Fe)作为基体并经时效处理后,α-Fe(Ni,Al)析出相对NiAl(Fe)有时效硬化作用,含有α-Fe(Ni,Al)析出相的NiAl(Fe)在所有实验温度区域内.其屈服强度均远高于单相NiAl的屈服强度.透射电镜的观察揭示出α-Fe(Ni,Al)析出相为体心立方结构,时效初期是球状,相邻析出相合并变成板条状,平行于有序基体的{100}晶面析出.当以α-Fe(Ni,Al)相为基体进行时效处理后,NiAl(Fe)析出相对α-Fe(Ni,Al)也起到了析出强化的作用.通过透射电镜的观察可知,NiAl(Fe)析出相的形态在时效初期时呈球状,随着时效时间的延长,析出相会长大并呈四方六面体,但相邻析出相之间不会合并.
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