以(R,R)-1,2-二苯基乙二醇和氰尿酰氯为原料,经保护、醚化、去保护、取代等反应合成了一种新的手性多齿配体2-乙氧基-4-(2-甲氧基-乙氧基)-6-((1R,2R)-1,2-二苯基-2-甲氧基-乙氧基)-1,3,5-三嗪,并通过1H NMR、LCMS和元素分析测试技术对目标化合物的结构进行了表征.
A novel chiral polydentate ligand, 2-ethoxy-4-(2-methoxy-ethoxy)-6-((1R,2R)-1 ,2-diphenyl-2-methoxy-ethoxy)-1 ,3 ,5-triazine, was synthesized from ( R, R) -hydrobenzoin and cyanuric chloride by means of functional group prelection, etherification, deprotection and substitution. The structure of the target product was characterized by ~1H NMR, LCMS and elemental analysis.
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