羟基磷灰石是一种最有发展前途的生物材料之一.采用电泳沉积方法在钛合金基体上制备了HA/TiO2生物陶瓷涂层.将HA和TiO2粉体分散到正丁醇溶液中,再加入三乙醇胺,通过zeta电位确定了稳定的悬浮液中三乙醇胺和HA/TiO2的含量.研究了沉积电压和电泳时间对HA/TiO2涂层形貌和沉积量的影响.制得均匀致密涂层的适宜电压范围为250～350V.研究结果表明:由于电场强度随沉积时间改变,HA/TiO2沉积量随着沉积时间的增加表现出2段沉积速率不同的线性增长.
参考文献
| [1] | Dasarathy H;Riley C;Coble H D.Analysis of apatite deposits on substrates[J].Journal of Biomedical Materials Research,1993(27):477-482. |
| [2] | Currey J.Biomaterials:sacrificial bonds heal bone[J].Nature,2001(414):699-708. |
| [3] | Yildirim OS;Aksakal B;Celik H;Vangolu Y;Okur A .An investigation of the effects of hydroxyapatite coatings on the fixation strength of cortical screws.[J].Medical engineering and physics,2005(3):221-228. |
| [4] | 黄紫洋,刘榕芳,肖秀峰.电泳沉积羟基磷灰石生物陶瓷涂层的研究进展[J].硅酸盐学报,2003(06):591-597. |
| [5] | Ng BS;Annergren I;Soutar AM;Khor KA;Jarfors AE .Characterisation of a duplex TiO(2)/CaP coating on Ti6Al4V for hard tissue replacement.[J].Biomaterials,2005(10):1087-1095. |
| [6] | Kim HW;Koh YH;Li LH;Lee S;Kim HE .Hydroxyapatite coating on titanium substrate with titania buffer layer processed by sol-gel method.[J].Biomaterials,2004(13):2533-2538. |
| [7] | Xiao XF;Liu RF;Zheng YZ .Characterization of hydroxyapatite/titania composite coatings codeposited by a hydrothermal-electrochemical method on titanium[J].Surface & Coatings Technology,2006(14/15):4406-4413. |
| [8] | Tomaszek R;Pawlowski L;Gengembre L;Laureyns J;Le Maguer A .Microstructure of suspension plasma sprayed multilayer coatings of hydroxyapatite and titanium oxide[J].Surface & Coatings Technology,2007(16/17):7432-7440. |
| [9] | 徐益,秦传江,赵柏森,黄楠.钛基羟基磷灰石涂层的界面结构及梯度设计[J].表面技术,2005(01):58-61. |
| [10] | 康健强,吴慧敏,李卫东,左正忠.电化学方法制备生物活性陶瓷[J].电镀与精饰,2004(01):18-22,30. |
| [11] | 卢立柱,胡湖生,谢慧琴,李凌川.电泳沉积法制备固体电解质薄膜的沉积速率和沉积机理[J].化工冶金,1998(02):97-103. |
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