制备了锌/富勒醇复合材料并研究了富勒醇对复合材料性能的影响.锌/富勒醇复合材料的制备分两步进行,其中包括电沉积制备富勒醇薄膜和电镀金属锌.采用辉光放电光谱法对富勒醇在镀层中的分布进行了表征.通过对锌/富勒醇复合材料硬度、耐盐雾腐蚀、交流阻抗谱和减摩性测试,分析了富勒醇对复合材料性能的影响.结果表明:富勒醇在锌/富勒醇复合材料中的分布不均匀;富勒醇对锌镀层的硬度、耐蚀性以及自润滑性都有不同程度的影响.
参考文献
| [1] | Chiang LY;Wang LY;Swirczewski JW et al.Efficient Synthesis of Polyhydroxylated Fullerene Derivatives via Hydrolysis of Polycyclosulfated Precursors[J].Organic Chemistry,1994,59:3960-3968. |
| [2] | Kokubo, K.;Matsubayashi, K.;Tategaki, H.;Takada, H.;Oshima, T. .Facile synthesis of highly water-soluble fullerenes more than half-covered by hydroxyl groups[J].ACS nano,2008(2):327-333. |
| [3] | Troshin, PA;Astakhova, AS;Lyubovskaya, RN .Synthesis of fullerenols from halofullerenes[J].Fullerenes, Nanotubes, and Carbon Nanostructures,2005(4):331-343. |
| [4] | Alves GC;Ladeira LO;Righi A;Krambrock K;Calado HD;Gil RPDF;Pinheiro MVB .Synthesis of C-60(OH)(18-20) in aqueous alkaline solution under O-2-atmosphere[J].Journal of the Brazilian Chemical Society,2006(6):1186-1190. |
| [5] | Lars O.Husebo;Balaji Sitharaman;Ko Furukawa;Tatsuhisa Kato;Lon J.Wilson .Fullerenols Revisited as Stable Radical Anions[J].Journal of the American Chemical Society,2004(38):12055-12064. |
| [6] | Robin Anderson;Andrew R.Barron .Reaction of Hydroxyfullerene with Metal Salts:A Route to Remediation and Immobilization[J].Journal of the American Chemical Society,2005(30):10458-10459. |
| [7] | Wang, F.F.;Li, N.;Tian, D.;Xia, G.F.;Xiao, N. .Efficient synthesis of fullerenol in anion form for the preparation of electrodeposited films[J].ACS nano,2010(10):5565-5572. |
上一张
下一张
上一张
下一张
计量
- 下载量()
- 访问量()
文章评分
- 您的评分：
-
10%
-
20%
-
30%
-
40%
-
50%