材料工程, 2000, (3): 36-38. doi: 10.3969/j.issn.1001-4381.2000.03.010
燃烧合成AlN/ Y2O3陶瓷及致密化机理分析
郑永挺 1, , 韩杰才 2, , 张幸红 {"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"HT9钢在核反应堆包壳管中具有巨大的应用前景.在失水事故下,包壳管材料的温度将远高于600℃.为此,研究了HT9钢600℃以上的空气氧化行为.用增重法测定其氧化动力学曲线,利用SEM、EDS和XRD分析氧化产物的形貌、成分和结构.基于对氧化动力学与氧化产物的分析,探讨其氧化机制.结果表明:在600~1000℃范围内随着温度的升高和时间的延长,HT9钢氧化程度增加;氧化层呈双层结构,内层为(Fe,Cr)2 O3,外层是Fe2 O3;不同温度的氧化动力学遵循不同的规律,氧化过程主要受铁离子和铬离子的扩散共同控制.","authors":[{"authorName":"赵蒙蒙","id":"7d9598b6-07b5-4cbb-951e-64f626055e4e","originalAuthorName":"赵蒙蒙"},{"authorName":"张程煜","id":"87b3f691-ec12-405a-b4dc-54127688ef62","originalAuthorName":"张程煜"},{"authorName":"李丽华","id":"e2bc3581-8d32-4ab7-bcd4-86ec3f02914c","originalAuthorName":"李丽华"},{"authorName":"唐睿","id":"aa02639d-6ee7-4c02-a342-5e2fd0a89b65","originalAuthorName":"唐睿"},{"authorName":"陈乐","id":"d2cfc875-8d33-4f6d-b0ed-9754bc24c439","originalAuthorName":"陈乐"}],"doi":"10.13228/j.boyuan.issn1001-0963.20140276","fpage":"317","id":"ca6ac0ff-58a2-41bf-ae00-64d6aaa93e75","issue":"4","journal":{"abbrevTitle":"GTYJXB","coverImgSrc":"journal/img/cover/GTYJXB.jpg","id":"30","issnPpub":"1001-0963","publisherId":"GTYJXB","title":"钢铁研究学报"},"keywords":[{"id":"7554b54b-ba02-4a88-a1c5-c5f32e8247b0","keyword":"HT9钢","originalKeyword":"HT9钢"},{"id":"e0c32993-f4de-4de2-b2b7-10915294951e","keyword":"空气氧化","originalKeyword":"空气氧化"},{"id":"bf99f6a2-07a2-40ee-be23-e0956edfa131","keyword":"氧化动力学","originalKeyword":"氧化动力学"},{"id":"14136a61-0f47-4a5c-85ae-dd8995e8377d","keyword":"氧化层","originalKeyword":"氧化层"}],"language":"zh","publisherId":"gtyjxb201704012","title":"核包壳管用HT9钢的600~1000℃空气氧化行为","volume":"29","year":"2017"},{"abstractinfo":"对高拉力钢HT60的腐蚀疲劳裂纹扩展特性和门槛值区域特性,采用紧凑拉伸试件在人工海水中进行了实验和研究,结果表明:在空气中的da/dN与ΔK_(cff)关系可以作为在海水中的da/dN与ΔK关系的一个偏保守的预测;在高应力比的高ΔK区域,由于应力诱起溶解促进了裂纹扩展的加速;该裂纹开口应力强度因子K_(op)仅反映了裂纹表面同腐蚀生成物接触的结果,从而导致了K_(op)在裂纹尖端的偏大的估计结果。","authors":[{"authorName":"高鸿斌","id":"7c42b2d6-68cc-4e4b-b2b6-c4dfe54befea","originalAuthorName":"高鸿斌"}],"categoryName":"|","doi":"","fpage":"121","id":"9a745675-bea7-47b9-b46b-1a7bbc14ca7c","issue":"4","journal":{"abbrevTitle":"JSXB","coverImgSrc":"journal/img/cover/JSXB.jpg","id":"48","issnPpub":"0412-1961","publisherId":"JSXB","title":"金属学报"},"keywords":[{"id":"455aaad1-89b5-407e-9b11-a47a6c97c723","keyword":"腐蚀疲劳","originalKeyword":"腐蚀疲劳"},{"id":"3db8f73e-3135-415c-b32f-9dc7f9549db4","keyword":"crack growth","originalKeyword":"crack growth"},{"id":"cea978ee-b77c-49df-b0d4-139af401d96c","keyword":"crack closure","originalKeyword":"crack closure"},{"id":"8a4f32a3-ff43-45fe-bda5-97db7e251e0f","keyword":"synthetic sea water","originalKeyword":"synthetic sea water"}],"language":"zh","publisherId":"0412-1961_1991_4_17","title":"HT60高拉力钢在人工海水中的腐蚀疲劳裂纹扩展特性","volume":"27","year":"1991"},{"abstractinfo":"对QLT处理后的9%Ni钢在室温和低温下进行拉伸试验，采用X射线法对拉伸前后样品中的奥氏体含量进行了测试，利用透射分析拉伸试样断口附近的显微组织，研究了低温拉伸过程中逆转变奥氏体/马氏体对QLT处理9%Ni钢拉伸变形行为的影响。研究表明：QLT处理9%Ni钢在20~-196℃系列温度拉伸时，随试验温度的降低，强度和均匀伸长率均提高、屈强比降低。逆转变奥氏体在拉伸时发生相变而改善了9%Ni钢的低温塑性。","authors":[{"authorName":"苏航，赵希庆，潘涛，高建忠，王青峰","id":"1b24d8dc-00f3-4014-bd24-7e93b5309d4f","originalAuthorName":"苏航，赵希庆，潘涛，高建忠，王青峰"}],"categoryName":"|","doi":"","fpage":"55","id":"23a31373-3ce4-4294-af40-7d6f6a5f5062","issue":"7","journal":{"abbrevTitle":"GT","coverImgSrc":"journal/img/cover/GT.jpg","id":"27","issnPpub":"0449-749X","publisherId":"GT","title":"钢铁"},"keywords":[{"id":"c0f9c620-79d0-4926-8c48-f4f467dcf1d5","keyword":"9%Ni低温钢 ","originalKeyword":"9%Ni低温钢 "},{"id":"d425df97-1a5d-42b6-b9a5-fe1bf052814e","keyword":" QLT treatment ","originalKeyword":" QLT treatment "},{"id":"57283d7e-a8b1-407f-9f6a-46ddf29cf139","keyword":" reversed austenite ","originalKeyword":" reversed austenite "},{"id":"a7e157f2-74ab-4b6b-a6ba-3a9bb74b717e","keyword":" cryogenic toughness","originalKeyword":" cryogenic toughness"}],"language":"zh","publisherId":"0449-749X_2012_7_16","title":"QLT处理9%Ni钢低温拉伸性能的研究","volume":"47","year":"2012"},{"abstractinfo":"对QLT处理后的9%Ni钢在室温和低温下进行拉伸试验,采用X射线法对拉伸前后样品中的奥氏体含量进行了测试,利用透射分析拉伸试样断口附近的显微组织,研究了低温拉伸过程中逆转变奥氏体/马氏体对QLT处理9%Ni钢拉伸变形行为的影响。研究表明：QLT处理9%Ni钢在20～-196℃系列温度拉伸时,随试验温度的降低,强度和均匀伸长率均提高、屈强比降低。逆转变奥氏体在拉伸时发生相变而改善了9%Ni钢的低温塑性。","authors":[{"authorName":"苏航","id":"5f5b2585-c5fa-47ef-b1e7-3fdb61b622bb","originalAuthorName":"苏航"},{"authorName":"赵希庆","id":"6004f24b-f716-47a1-bab4-4ee6504174fd","originalAuthorName":"赵希庆"},{"authorName":"潘涛","id":"a753106f-d67f-43cf-818b-797528a7059d","originalAuthorName":"潘涛"},{"authorName":"高建忠","id":"6741c08b-6df3-413b-bfb2-92f15bc4ebd7","originalAuthorName":"高建忠"},{"authorName":"王青峰","id":"791ac576-bbdb-43e8-8609-f2a642247e4d","originalAuthorName":"王青峰"}],"doi":"","fpage":"55","id":"ce08faa3-fc7c-466e-99ab-3e3ff6961c79","issue":"7","journal":{"abbrevTitle":"GT","coverImgSrc":"journal/img/cover/GT.jpg","id":"27","issnPpub":"0449-749X","publisherId":"GT","title":"钢铁"},"keywords":[{"id":"8e12ab4c-4d13-4de3-8276-8c5d32189a3f","keyword":"9％Ni低温钢","originalKeyword":"9％Ni低温钢"},{"id":"3ba58404-5ff7-4826-86cf-7f55d4211b21","keyword":"QLT处理","originalKeyword":"QLT处理"},{"id":"4216a591-4296-4372-a412-6ab086fdd299","keyword":"逆转变奥氏体","originalKeyword":"逆转变奥氏体"},{"id":"813a43da-5c4a-422c-8b5a-ae58bc1bb7e5","keyword":"低温韧性","originalKeyword":"低温韧性"}],"language":"zh","publisherId":"gt201207012","title":"QLT处理9%Ni钢低温拉伸性能的研究","volume":"47","year":"2012"},{"abstractinfo":"为提高31CrMoV9钢的综合力学性能，对其进行调质处理工艺研究。对材料的力学性能和组织进行分析，确定调质工艺为淬火温度(900±10) ℃，回火温度635 ℃。调质处理后，材料的力学性能完全满足标准要求。","authors":[{"authorName":"刘金鑫，冯桂萍，王连海","id":"9f39c795-b829-4657-9134-368bf5216f4c","originalAuthorName":"刘金鑫，冯桂萍，王连海"}],"categoryName":"|","doi":"","fpage":"17","id":"86260148-5121-444c-945e-c146cad106b1","issue":"2","journal":{"abbrevTitle":"WLCS","coverImgSrc":"journal/img/cover/WLCS.jpg","id":"64","issnPpub":"1001-0777","publisherId":"WLCS","title":"物理测试"},"keywords":[{"id":"24e50707-61f6-486f-b692-603becd25c04","keyword":"31CrMoV9钢","originalKeyword":"31CrMoV9钢"},{"id":"6fbf4193-85f4-4809-b5fc-57bb4d1fd99e","keyword":"quenchingandtempering","originalKeyword":"quenchingandtempering"},{"id":"349cdfef-fea8-440d-88eb-44784f5bbab7","keyword":"property","originalKeyword":"property"},{"id":"c00ae969-3821-4900-80e2-ef21eee7d6b7","keyword":"structure","originalKeyword":"structure"}],"language":"zh","publisherId":"1001-0777_2011_2_10","title":"31CrMoV9钢调质工艺研究","volume":"29","year":"2011"},{"abstractinfo":"为提高31CrMoV9钢的综合力学性能,对其进行调质处理工艺研究.对材料的力学性能和组织进行分析,确定调质工艺为淬火温度(900±10)℃,回火温度635℃.调质处理后,材料的力学性能完全满足标准要求.","authors":[{"authorName":"刘金鑫","id":"7e3a0eb1-85db-4903-b9db-38adc1a045e4","originalAuthorName":"刘金鑫"},{"authorName":"冯桂萍","id":"ad980831-9a0a-4472-a301-03e99114e592","originalAuthorName":"冯桂萍"},{"authorName":"王连海","id":"284fd07a-28b7-4a2c-b7ce-38af0042f261","originalAuthorName":"王连海"}],"doi":"","fpage":"17","id":"a22dccc1-47d0-4abe-bf66-6217e691aac4","issue":"2","journal":{"abbrevTitle":"WLCS","coverImgSrc":"journal/img/cover/WLCS.jpg","id":"64","issnPpub":"1001-0777","publisherId":"WLCS","title":"物理测试"},"keywords":[{"id":"e6c60d66-6576-4840-8e3f-808a49ed3375","keyword":"31CrMoV9钢","originalKeyword":"31CrMoV9钢"},{"id":"346ba282-13b5-41c5-bedb-a74fe451496f","keyword":"调质","originalKeyword":"调质"},{"id":"3b63c8f0-409e-48af-84bc-5ae0c0073823","keyword":"性能","originalKeyword":"性能"},{"id":"ec4f2d01-2b88-41cc-b39e-c5cd1516e469","keyword":"组织","originalKeyword":"组织"}],"language":"zh","publisherId":"wlcs201102004","title":"31CrMoV9钢调质工艺研究","volume":"29","year":"2011"},{"abstractinfo":" 针对国产9Ni钢，对其进行焊接及热处理工艺制定。采用多层多道手工电弧焊，焊条为ENiCrMo-3，焊前不预热且严格控制层间温度；选择双相区处理工艺。通过高低温拉伸试验、低温冲击试验、硬度测试及金相组织观察检测焊接接头性能。结果表明，9Ni钢接头低温冲击韧性和抗拉强度均满足要求，对其制定的焊接和热处理工艺切实可行。","authors":[{"authorName":"张敏","id":"0338ae38-878d-4485-9d8f-6f9088ada502","originalAuthorName":"张敏"},{"authorName":"褚巧玲","id":"f4919895-3898-4428-b93d-5ef21420f5d6","originalAuthorName":"褚巧玲"},{"authorName":"李继红","id":"1e9d0c45-ffcc-42fd-862d-03099083a6dd","originalAuthorName":"李继红"}],"doi":"","fpage":"10","id":"f9d7d393-479b-479c-a923-840df029a727","issue":"4","journal":{"abbrevTitle":"BQCLKXYGC","coverImgSrc":"journal/img/cover/BQCLKXYGC.jpg","id":"4","issnPpub":"1004-244X","publisherId":"BQCLKXYGC","title":"兵器材料科学与工程 "},"keywords":[{"id":"d792eda6-26e6-4a79-adb1-a0d86a11947a","keyword":"9Ni钢","originalKeyword":"9Ni钢"},{"id":"0cae064d-d06d-4191-9cd5-cdd0c23a673e","keyword":"焊接接头","originalKeyword":"焊接接头"},{"id":"e9210839-90ff-43de-b67d-618859157c6f","keyword":"低温冲击韧性","originalKeyword":"低温冲击韧性"},{"id":"3990b663-972f-48d5-b0c0-b42ac834ca2a","keyword":"双相区处理","originalKeyword":"双相区处理"}],"language":"zh","publisherId":"bqclkxygc201304003","title":"9Ni钢焊接接头低温性能研究","volume":"","year":"2013"},{"abstractinfo":"本文对利用雾化法直接制备出Y、Ti过饱和固溶的粉体合金,经短时机械合金化和热等静压成型制备纳米结构9Cr-ODS钢技术进行了研究.采用扫描电镜和X射线衍射研究雾化合金粉与短时球磨后雾化合金粉的形貌特征与组织的演化.通过高分辨透射电镜和电子背散射衍射研究热固化成型后ODS钢的微观组织.测试了雾化粉和球磨8h合金粉热固化成型样品的应力-应变曲线.结果表明,用短时球磨雾化粉制备的ODS钢晶粒尺寸更加细小、形成高密度纳米尺寸的析出相.与常规方法制备的ODS钢相比,抗拉强度略高、塑性显著提高、球磨时间大幅缩短.","authors":[{"authorName":"吕铮","id":"b37aec16-3028-4d1f-8a25-546cffd4d2c0","originalAuthorName":"吕铮"},{"authorName":"胡彭浩","id":"31025452-7fd2-49b2-88cb-1e05a51ebef6","originalAuthorName":"胡彭浩"},{"authorName":"张国玉","id":"75cbd793-a9ed-4cef-ab9b-00acb4a507f9","originalAuthorName":"张国玉"},{"authorName":"田利","id":"8cdb4819-5146-478d-b18d-3bf8c09286fc","originalAuthorName":"田利"}],"doi":"10.14186/j.cnki.1671-6620.2015.01.014","fpage":"67","id":"f35310d4-fdc6-4a12-a971-046ecca91aea","issue":"1","journal":{"abbrevTitle":"CLYYJXB","coverImgSrc":"journal/img/cover/CLYYJXB.jpg","id":"17","issnPpub":"1671-6620","publisherId":"CLYYJXB","title":"材料与冶金学报"},"keywords":[{"id":"4492c7ae-9005-4694-aadb-345f0c57a43d","keyword":"ODS钢","originalKeyword":"ODS钢"},{"id":"dec3abb6-4c2c-483f-bc3b-fde163a7513e","keyword":"雾化","originalKeyword":"雾化"},{"id":"700858f6-fabc-440a-bb6b-61676d61b156","keyword":"球磨","originalKeyword":"球磨"},{"id":"f452c341-5e3e-4176-b901-fa36ef8b8b1d","keyword":"纳米析出相","originalKeyword":"纳米析出相"},{"id":"7228d1b3-e579-43ce-9de0-2d5480453008","keyword":"抗拉强度","originalKeyword":"抗拉强度"}],"language":"zh","publisherId":"clyyjxb201501014","title":"纳米结构9Cr-ODS钢的制备工艺","volume":"14","year":"2015"},{"abstractinfo":"31CrMoV9是欧洲牌号的高淬透性合金钢，属于近几年国产化过程中新研制的钢种。为比较国内外成品钢质量的差距，提高中国该钢种的冶炼水平，选取不同产地的31CrMoV9钢，对其中的非金属夹杂物进行研究。电解钢样观察其中夹杂物的外观形貌，并对钢样进行金相观察和利用高温共聚焦显微镜观察钢样的组织变化。研究发现，单一成分的夹杂物多为长条状，而复合夹杂物多为球形。研究过程所选取的中国生产的钢材与德国钢材在夹杂物的数量和形态控制上存在差距，中国生产的钢材单位面积内夹杂物的数量更多，夹杂物的大小不均匀，形态控制不理想。就成分而言，德国钢材的夹杂物成分主要是以Al2O3、CaO、MnS等组成的复合夹杂物，而中国钢材的夹杂物存在着成分的波动性。共聚焦显微镜试验过程中发现，在升温过程中夹杂物会发生球化现象，降温过程中，钢样开始形成马氏体组织的温度有所不同，中国钢样为580℃，德国钢样为450℃，这与其本身晶体的成分有关，最后的组织为马氏体+碳化物颗粒+残余奥氏体。","authors":[{"authorName":"何志军","id":"41abf9ae-0aeb-4c95-8f74-087117ce764c","originalAuthorName":"何志军"},{"authorName":"戴雨翔","id":"f924b0b2-8f74-4df2-8fde-67253a57c206","originalAuthorName":"戴雨翔"},{"authorName":"刘吉辉","id":"1b6ec7ca-18b7-43e5-a396-7dde74736342","originalAuthorName":"刘吉辉"},{"authorName":"庞清海","id":"acbe4f7a-f850-48d6-9372-7111016d16fc","originalAuthorName":"庞清海"},{"authorName":"赵啸","id":"b8e623f2-eaa1-49a9-a813-79aa800a8ef8","originalAuthorName":"赵啸"},{"authorName":"湛文龙","id":"2ac5df57-4ad9-428f-a965-305137026646","originalAuthorName":"湛文龙"}],"doi":"10.13228/j.boyuan.issn0449-749x.20150611","fpage":"81","id":"c5a0302d-ebcb-46ea-a38b-dcd206d53b1c","issue":"7","journal":{"abbrevTitle":"GT","coverImgSrc":"journal/img/cover/GT.jpg","id":"27","issnPpub":"0449-749X","publisherId":"GT","title":"钢铁"},"keywords":[{"id":"d0ffdca9-f60b-4266-821f-e125738366c4","keyword":"31CrMoV9","originalKeyword":"31CrMoV9"},{"id":"67d6de58-2cc5-44fa-837a-7091fd3ad511","keyword":"非金属夹杂物","originalKeyword":"非金属夹杂物"},{"id":"44bcfccd-6066-48d2-8187-fb20fa9eda58","keyword":"组织结构","originalKeyword":"组织结构"},{"id":"d97871d6-022b-45a2-a0ad-49703d31dd88","keyword":"高温共聚焦显微镜","originalKeyword":"高温共聚焦显微镜"}],"language":"zh","publisherId":"gt201607015","title":"31CrMoV9钢夹杂物和组织观察","volume":"51","year":"2016"},{"abstractinfo":"利用ＴＥＭ研究了Ｎｉ９钢中马氏体与奥氏体的微观结构。结果表明，多数回火奥氏体不是严格地按Ｋ－Ｓ或Ｎ－Ｗ关系析出，而是在这两种取向附近变化：在同一马氏体束内，奥氏体可按上述近似关系的不同变体析出；回火奥氏体主药第马氏体晶界析出，呈板条状，惯习面为（３３５）（γ＇）∥（３４１）α，奥氏体向马氏体转变时易形成马氏体孪晶，这些孪晶在随后的回火过程中消失","authors":[{"authorName":"李光来","id":"86963ba7-b74d-4a15-a5a1-2b676ac37cac","originalAuthorName":"李光来"},{"authorName":"孟祥敏","id":"6249c229-ebc9-41a6-85c3-4900d844874f","originalAuthorName":"孟祥敏"},{"authorName":"张弗天","id":"982bcf8c-ef58-4d2b-940e-5a91ee6610d5","originalAuthorName":"张弗天"},{"authorName":"吴玉琨","id":"451cea0e-3bda-4c4a-b937-92b76c8e6685","originalAuthorName":"吴玉琨"}],"categoryName":"|","doi":"","fpage":"1121","id":"9bedfdf1-5e9c-4699-9c4f-8fc1dfb9c027","issue":"11","journal":{"abbrevTitle":"JSXB","coverImgSrc":"journal/img/cover/JSXB.jpg","id":"48","issnPpub":"0412-1961","publisherId":"JSXB","title":"金属学报"},"keywords":[{"id":"10774fa6-88cc-49d4-b4fc-c715b7189191","keyword":"Ｎｉ９钢","originalKeyword":"Ｎｉ９钢"},{"id":"4312ecbd-4514-4af7-967e-d3c90f347612","keyword":" martensite","originalKeyword":" martensite"},{"id":"ccffb839-c175-4e7d-911c-ad674256d1c3","keyword":" austenite","originalKeyword":" austenite"},{"id":"4a3c102f-3071-496c-b7a4-8435bd163da4","keyword":" microstructure","originalKeyword":" microstructure"}],"language":"zh","publisherId":"0412-1961_1996_11_6","title":"Ni9钢微观结构的TEM研究","volume":"32","year":"1996"}],"totalpage":2876,"totalrecord":28755}