以固态氧化物为原料,采用二次合成工艺制备PMS-PZT三元系压电陶瓷.研究组成为Pb1.04(Mn1/3Sb2/3)0.05ZrxTi0.95-xO3的压电陶瓷的相组成、显微结构、电性能以及温度稳定性.结果表明:合成温度900℃保温2h,可以得到钙钛矿结构.烧结温度1240℃保温2h时,综合性能达最佳值:εT33/ε0=1420,d33=324pC/N,Kp=62%,Qm=2400,tanδ=0.0029.烧成温度影响谐振频率的变化率.提高烧成温度可以使正温范围的变化率提高,负温范围的变化率降低.
参考文献
| [1] | Cheol-Su Kim;Seong-Kon Kim;Sang Yeol Lee .Piezoelectric properties of new PZT-PMWSN ceramic[J].Materials Letters,2003(15):2233-2237. |
| [2] | C.Galassi;F.Craciun .Processing and characterization of high Qm ferroelectric ceramics[J].Journal of the European Ceramic Society,1999(6/7):1237-1241. |
| [3] | KIM S K;KIM C S .Piezoelectric and electrical properties of PZT-PSN thin film ceramic for MEMS applications[J].Materials Science in Semiconductor Processing,2003,5(02):115-121. |
| [4] | Chen HY.;Guo XB.;Meng ZY. .Processing and properties of PMMN-PZT quaternary piezoelectric ceramics for ultrasonic motors[J].Materials Chemistry and Physics,2002(1/3):202-206. |
| [5] | LONG J W;MENG Z Y .Effect of ratio the properties of PMMN-PZT ceramics near the morphotropic phase boundary[J].Materials Science and Engineering B,2003,99:433-436. |
| [6] | Jiwen Long;Haiyan Chen;Zhongyan Meng .Effects of compositions and Nb-doping on microstructure and piezoelectric properties of PMS-PZ-PT system[J].Materials Science & Engineering, B. Solid-State Materials for Advanced Technology,2003(1/3):445-448. |
| [7] | Yoon SJ.;Kucheiko SI.;Kim HJ.;Jung HJ.;Lee DK.;Ahn HK.;Kang HW. .Piezoelectric properties of Pb[Zr0.45Ti0.5-xLux(Mn1/3Sb2/3)(0.05)]O-3 ceramics[J].Journal of the American Ceramic Society,1998(9):2473-2476. |
| [8] | 郭晓波,陈海,孟中岩.Pb 1-xSrx（Mn1/3Sb2/3）aZrbTicO3三元系压电陶瓷的压电和介电性能[J].硅酸盐学报,2002(01):125-127. |
| [9] | SEND T;BRADT R C .Grain growth in sintered ZnO and ZnO-Bi2O3 ceramics[J].Journal of the American Ceramic Society,1990,71:106-144. |
| [10] | Wang MC.;Huang MS.;Wong TS.;Wu NC. .Sintering and piezoelectric properties of Pb(Ni1/3Sb2/3)O-3-PbZrO3-PbTiO3 ceramics[J].Journal of Materials Science,2002(3):663-668. |
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