欢迎登录材料期刊网

材料期刊网

高级检索

采用离子辅助增强磁控溅射与离子蒸发镀二元组合源设备在高速钢基体沉积出微量 Al 掺杂的TiN涂层(Al-TiN),利用扫描电子显微镜、X射线衍射仪、显微硬度计对涂层的组成成分、相结构、膜基结合力及显微硬度进行了分析;用摩擦磨损实验机及台阶仪分析了薄膜的摩擦磨损性能。研究了微量 Al 掺杂对薄膜的微结构及性能的影响。结果表明,TiN 涂层中微量Al的存在使涂层的膜基结合力、耐摩擦磨损性能得到明显改善。

Al-TiN coating deposited on high speed steel by plasma enhanced magnetron sputtering ion plating and evaporating deposition combination sources equipment.Study on the effect of little Al doped on the micro-structure and mechanical properties of TiN coating.The elements,phase structure,film-substrate cohesion and microhardness were characterized by scanning electron microscopy (SEM),X-ray diffraction (XRD),micro-hardness meter;the wear resistance was investigated with CSEM pin-on-disk wear test apparatus and step profi-ler.The results show that the addition of little Al make the film-substrate cohesion and wear resistance are evi-dently improved.

参考文献

[1] M. Hua;H. Y. Tam;H. Y. Ma;C. K. Mok .Patterned PVD TiN spot coatings on M2 steel: Tribological behaviors under different sliding speeds[J].Wear: an International Journal on the Science and Technology of Friction, Lubrication and Wear,2006(11/12):1153-1165.
[2] Santner E;Klaffke D;Kijcker G M .Comprehensive tri-bological characterization of thin TiN-based coatings[J].WEAR,1995,190:204-211.
[3] 陈利,汪秀全,尹飞,李佳.TiN涂层的微观组织结构及力学性能分析[J].硬质合金,2006(01):8-10.
[4] Yoon S Y;Kim J K;HoKim K .A comparative study on tribological behavior of TiN and TiAlN coatings prepared by arc ion plating technique[J].Surface and Coatings Technology,2002,161:237-242.
[5] 顾艳红,王成彪,刘家浚.氮化钛铝薄膜的制备及其摩擦学性能的研究[J].中国表面工程,2004(05):33-37.
[6] Lewis D B;Donohue L A.The influence of the yttrium content on the structure and properties of Ti1-x-y-z Alx Cry Yz N PVD hard coatings[J].Surface and Coatings Technology,1999(114):187-199.
[7] Yoon SY.;Chung WS.;Kim KH. .Impact-wear behaviors of TiN and Ti-Al-N coatings on AISI D2 steel and WC-Co substrates[J].Surface & Coatings Technology,2004(0):645-650.
[8] Polini R;Mantini FP;Braic M;Amar M;Ahmed W;Taylor H .Effects of Ti- and Zr-based interlayer coatings on the hot filament chemical vapour deposition of diamond on high speed steel[J].Thin Solid Films: An International Journal on the Science and Technology of Thin and Thick Films,2006(1/2):116-122.
[9] Cai ZH;Zhang P;Tan J .Adhesion improvement of cubic boron nitride film on high speed steel substrate by BNX implanted buffer interlayer[J].Surface & Coatings Technology,2007(15):6723-6725.
[10] J. Gerth;U. Wiklund .The influence of metallic interlayers on the adhesion of PVD TiN coatings on high-speed steel[J].Wear: an International Journal on the Science and Technology of Friction, Lubrication and Wear,2008(9/10):885-892.
[11] 弓满锋,乔生儒,卢国锋,姬浩.X射线测量高速钢上不同厚度氮化钛涂层残余应力[J].材料科学与工艺,2010(03):415-419,424.
[12] 吴劲峰,何乃如,邱孟柯,吉利,李红轩,黄小鹏.N2流量对中频非平衡磁控溅射TiAlN薄膜结构及性能的影响[J].功能材料,2013(01):32-35.
[13] 刘天伟,鲜晓斌,武胜,董闯.不同偏压下铀表面多弧离子镀TiN薄膜性能研究[J].稀有金属材料与工程,2006(09):1437-1440.
[14] Chicot D.;Lesage J. .ABSOLUTE HARDNESS OF FILMS AND COATINGS[J].Thin Solid Films: An International Journal on the Science and Technology of Thin and Thick Films,1995(1/2):123-130.
[15] 罗飞,何欣,杨会生,高克玮,王燕斌.溅射工艺对TiAlN薄膜摩擦学性能的影响[J].航空材料学报,2007(02):33-36.
[16] Seog-Young Yoon;Kwang O Lee;Sung Soo Kang .Comparison for mechanical properties between TiN and TiAlN coating layers by AIP technique[J].Journal of Materials Processing Technology,2002(0):260-265.
[17] ZHAO Hui,WANG Xiao-hui,LIU Qiu-lei,CHEN Li-jia,LIU Zheng.Structure and wear resistance of TiN and TiAlN coatings on AZ91 alloy deposited by multi-arc ion plating[J].中国有色金属学报(英文版),2010(z2):679-682.
[18] DD CEN/TS 1071-8.Rockwell indentation test for eval-uation of adhesion[S].
上一张 下一张
上一张 下一张
计量
  • 下载量()
  • 访问量()
文章评分
  • 您的评分:
  • 1
    0%
  • 2
    0%
  • 3
    0%
  • 4
    0%
  • 5
    0%