Fe73.5 Cu1 Nb3 Si13.5 B9纳米晶带材具有优异的软磁性能，在开关电源等领域得到广泛的应用，但Fe73.5 Cu1 Nb3 Si13.5 B9纳米晶带材磁芯在封装过程中存在着环氧树脂严重的不浸润问题，限制了纳米晶带材的应用。通过氧化处理法在带材表面制备了分布均匀、表面光洁、黑棕红色 Fe3 O4和 Fe2 O3氧化膜，氧化膜与带材结合力强，可以作为带材基体与环氧树脂的过渡层，改善了环氧树脂与带材的浸润性。相对于未表面氧化处理的带材，经过表面氧化处理带材的初始磁导率、饱和磁感应强度分别提高了14.6%和4.3%，矫顽力降低了21.6%。
Fe73.5 Cu1 Nb3 Si13.5 B9 nanocrystalline strip exhibit excellent soft magnetic properties,and was widely used in the field of switch power supply,etc.But Fe73.5 Cu1 Nb3 Si13.5 B9 nanocrystalline strip magnetic core exis-ted serious infiltration problem of epoxy resin in the process of encapsulation,which limited the application of nanocrystalline strip.We invest the oxidation process on the surface of the strip.The surface of the strip dis-tribute uniformity,smooth,dark red brown oxide film.With strong binding force with the strip,oxide film could be use as a transition layer of strip matrix and epoxy resin,so it could improve the infiltration between the strip and epoxy resin.Compared with the strip without surface oxidation treatment,the initial permeability and saturated magnetic induction intensity of the strip with surface oxidation treatment increased by 14.6% and 4. 3% respectively,and the coercive force was reduced by 2 1 .6%.
参考文献
| [1] | 杨操兵 .微量稀土La化的铁基非晶纳米晶带材的软磁及压磁特性研究[D].南昌大学,2010. |
| [2] | Savage S J;Froes F H .Production of rapidly solidified metals and alloys[J].Journal of Metals,1984,36:20-33. |
| [3] | 张甫飞,张洛,纪朝廉,李挹红,戴志华.纳米晶软磁合金材料及应用[J].上海金属,2002(01):21-26. |
| [4] | Shahria F;Beitollahia A;Shabestaria S G et al.Structural characterization and magnetoimpedance effect in amor-phous and nanocrystalline AlGe-substimted FeSiBNbCu ribbons[J].Journal of Magnetism and Magnetic Materi-als,2007,312:35-42. |
| [5] | Makino A;Inoue A;Masumoto T .Nanocrystalline soft magnetic Fe-MB(M=Zr,Hf,Nb)alloys produced by crystallization of amorphous phase[J].Materials transac-tions-JIM,1995,36:924-924. |
| [6] | A. Baron;D. Szewieczek;G. Nawrat .Corrosion of amorphous and nanocrystalline Fe-based alloys and its influence on their magnetic behavior[J].Electrochimica Acta,2007(18):5690-5695. |
| [7] | Lu Zhichao;Li Deren;Zhou Shaoxiong.Amorphous,nano-crystalline alloy development situation at home and abroad and application prospects[J].Advanced Materials Industry,2002(03):20-23. |
| [8] | Li Yaotian.Recent development on studies of nanocrys-talline soft magnetic alloys[J].Metallic Functional Mate-rials,1995(06):217. |
| [9] | 张甫飞,李挹红,纪朝廉,张洛.非晶微晶软磁合金系列电感材料及器件的开发应用[J].金属功能材料,2001(03):1-6. |
| [10] | 夏小鸽 .基于高性能非晶带材和磁芯封装的研究[D].南昌大学,2007. |
| [11] | 万珍珍,朱正吼,黄渝鸿.表面处理和温度对铁基非晶带材压磁性能的影响[J].功能材料,2008(06):942-945. |
| [12] | Zheng Ruiting.Discussion on high-temperature oxida-tion of steel parts[J].Electroplating & Pollution Con-trol,2003(01):26-29. |
| [13] | 张圣麟,陈华辉,李红玲,郑洪河,常照荣.常温磷化处理技术的研究现状及展望[J].材料保护,2006(07):42-47. |
| [14] | 余取民,李荣喜,许第发,宋勇.清洁型常温锌锰系磷化液研究[J].湘潭大学自然科学学报,2007(02):91-94. |
| [15] | Yu Qumin .Study on cleaning zinc-system phosphating solution at room temperature[J].Materials Protection,2006,39(05):26-28. |
| [16] | 余取民,李荣喜,卢红梅.钢铁表面免水洗锌系磷化膜的常温制备与性能表征[J].中南大学学报（自然科学版）,2008(05):940-944. |
| [17] | 李光玉,连建设,牛丽媛,江中浩,蒋青.AZ91D镁合金上钼改性锌系磷化膜的制备、结构及性能[J].高等学校化学学报,2006(05):817-820. |
- 下载量()
- 访问量()
- 您的评分：
-
10%
-
20%
-
30%
-
40%
-
50%