采用脉冲电沉积方法,在压缩机阀片表面制备Ni-SiC镀层。利用原子吸收分光光度计、透射电镜和硬度计研究脉冲电流密度对 Ni-SiC 镀层 SiC 粒子复合量、微观结构和显微硬度的影响。结果表明,随着脉冲电流密度的增大,Ni-SiC 镀层 SiC 粒子的复合量先增加后略有降低。在脉冲电流密度为7 A/dm2时,镀层SiC粒子的复合量高达9.92%(质量分数)。脉冲电流密度为7 A/dm2时,镀层致密、晶粒细小,SiC 粒子均匀分布于镀层中,且团聚现象较少。当脉冲电流密度为7 A/dm2时,镀层的显微硬度高达842.9 Hv。
Ni-SiC coatings were synthesized on the surface of compressor valves by using pulse electrodeposition method.The effect of current density on the content,microstructure and microhardness of the coatings was in-vestigated by using the atomic absorption spectrophotometer,transmission electron microscope and microhard-ness tester.The results show that the SiC particle content in the coating increases first and then decreases with the increase of pulse current density.The current density was 7 A/dm2 ,the coating has a density and fine structure,and SiC particles are evenly distributed in this coating.The current density was 7 A/dm2 ,the micro-hardness of the coating reaches 842.9 Hv.
参考文献
[1] | 王发辉,刘秀芳,程艳霞.往复压缩机故障诊断研究现状及展望[J].压缩机技术,2007(02):45-48. |
[2] | 郭磊.影响往复压缩机长周期运行的原因分析与解决措施[J].压缩机技术,2013(05):69-73. |
[3] | 王金东,代梅,夏法锋,李颖.压缩机阀片表面的超声-电沉积Ni-TiN镀层的工艺研究[J].兵器材料科学与工程,2013(03):55-56,57. |
[4] | Chunyang Ma;Guiqiang Liang;Yongyong Zhu .Preparation and corrosion assessment of electrodeposited Ni-SiC composite thin films[J].CERAMICS INTERNATIONAL,2014(2):3341-3346. |
[5] | Fafeng Xia;Chao Liu;Chunhua Ma .Preparation and corrosion behavior of electrodeposited Ni-TiN composite coatings[J].International Journal of Refractory Metals & Hard Materials,2012(Nov):295-299. |
[6] | 李超群,李新海,王志兴,郭华军.镀镍冲孔钢带的耐蚀性能和电化学机理研究[J].功能材料,2014(03):03042-03046. |
[7] | Xia Fafeng;Xu Huibin;Liu Chao et al.Microstructures of Ni-AlN composite coatings prepared by pulse electro-deposition technology[J].Applied Surface Science,2013,271:7-11. |
[8] | 胡振峰,汪笑鹤,吕镖,徐滨士.电流密度对自动化电刷镀Ni镀层组织结构和性能的影响[J].功能材料,2013(17):2507-2510. |
[9] | Xia, FF;Wu, MH;Wang, F;Jia, ZY;Wang, AL .Nanocomposite Ni-TiN coatings prepared by ultrasonic electrodeposition[J].Current applied physics: the official journal of the Korean Physical Society,2009(1):44-47. |
[10] | Ashassi-Sorkhabi H.;Rafizadeh SH. .Effect of coating time and heat treatment on structures and corrosion characteristics of electroless Ni-P alloy deposits[J].Surface & Coatings Technology,2004(3):318-326. |
- 下载量()
- 访问量()
- 您的评分:
-
10%
-
20%
-
30%
-
40%
-
50%