采用一步法制备了一种聚酰亚胺(PI)泡沫,研究了水含量对聚酰亚胺泡沫结构和性能的影响规律.采用红外光谱(FTIR)和扫描电镜(SEM)分别表征了聚酰亚胺泡沫的分子结构和泡孔结构;采用热机械分析(TMA)和热失重分析(TGA)分别测试了聚酰亚胺泡沫的玻璃化转变温度和热稳定性;采用双通道声学分析仪测试了聚酰亚胺泡沫的吸声性能.研究表明:在所研究的水含量范围内,用水含量对聚酰亚胺泡沫的分子结构、玻璃化转变温度和热失重性能几乎无影响;驻波管法测得PI泡沫的平均吸声系数最大为0.44;玻璃化转变温度为294.7~295.6℃,热失重5%时的温度大于377.5℃,800℃时的残余质量大于49.6%.
参考文献
[1] | 丁孟贤.聚酰亚胺:化学、结构与性能的关系及材料[M].北京:科学出版社,2006 |
[2] | SCHAUMBURG J G;RAYMOND LEE;USMON A K et al.Polyimide Foam[P].US,4355120,1982-10-19. |
[3] | CHOI K Y;LEE J H;LEE S G et al.Preparation of Polyimide Foam[P].US,6172127,2001-1-9. |
[4] | CHOI K Y;LEE J H;LEE S G et al.Method of Preparation Polyimide Foam with Excellent Flexibility Properties[P].US,6057379,2000-5-2. |
[5] | WEISER E S;NEWS N;CLAIR T S et al.Hollow Polyimide Microspheres[P].US,6235803,2001-5-22. |
[6] | WEISER E S;GRIMSLEY B W.Polyimide Foams from Friable Balloons[A].,2002:5,12-5,16. |
[7] | VAZQUEZ J M;CANO R J;JENSEN B J et al.Polyimide Foams[P].US,20060063848,2006-3-23. |
[8] | WERNSING D G;CLAYPOOL C J .Open Celled Low Density Foam and Method of Making such Open Celled Foam[P].US,5900440,1999-5-4. |
[9] | GMUNDEN W L;VOCKLABRUCK K W .Flame-retardant,High-temperature Resistant Foams of Polyimides[P].US,5153234,1992-10-6. |
[10] | RICCITIELLO S R;SAWKO P M;ESTRELLA C A .Catalysts for Polyimide Foams from Aromatic Isocyanates and Aromatic Dianhydrides[P].US,4177333,1979-12-4. |
[11] | ROSSER R W;CALIF S J;CLAYPOOL C J .Polyimide Foam for Thermal Insulation and Fire Protection[P].US,3772216,1973-11-13. |
[12] | 王连才;曾心苗;李淑风 等.一种聚酰亚胺泡沫及其制备方法[P].CN,200810227146.4,2008-11-25. |
[13] | 朱吕军;刘益军.聚氨酯泡沫塑料[M].北京:化学工业出版社,2005:22,24,31. |
上一张
下一张
上一张
下一张
计量
- 下载量()
- 访问量()
文章评分
- 您的评分:
-
10%
-
20%
-
30%
-
40%
-
50%