利用Al-Ti-TiO2体系原位反应合成了Nb掺杂Al2O3/TiAl复合材料.借助XRD和SEM研究了Nb掺杂Al2O3/TiAl的显微结构以及Nb引入量对复合材料显微结构的影响.结果表明,复合材料由TiAl、Ti3Al、Al2O3、Nb和NbAl3相构成,细小Al2O3颗粒分布于基体晶粒交界处,存在一定的团聚;Nb元素引入量的高低,可调节产物中TiAl和Ti3Al的相对含量,随Nb含量的增大,TiAl含量逐渐减少,Ti3Al则逐渐增大;同时,基体晶粒和Al2O3颗粒均有所细化,且分布逐渐均匀,材料的均匀性得到改善.
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