采用改进的HDDR工艺制备各向异性粘结NdFeB永磁材料,研究了Nd12.5Fe80.8B6.2Nb0.3Ga0.2(原子分数)合金氢化及脱氢制粉以及粘结磁体成形工艺.利用XRD、SEM及稀土永磁标准测量仪器等测试方法,对NdFeB合金材料吸氢-歧化反应以及脱氢过程中相变及微观组织进行观察分析,讨论了粘结成形工艺对磁体磁性能的影响.结果表明,Nd12.5Fe80.8B6.2Nb0.3Ga0.2合金低温吸氢并在820℃发生歧化反应,歧化相在820℃真空状态下重新再结合生成Nd2Fe14B硬磁相.通过精确控制反应过程中温度及氢气压力,可获得具有各向异性组织的NdFeB磁粉,结合合理的压制成形工艺条件,可制备出具有良好磁性能的粘结磁体.
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