欢迎登录材料期刊网

材料期刊网

高级检索

9,10-二[3,5-二(苯基)苯基]蒽是一种性能较好的小分子蓝色有机电致发光材料.通过改进的方法合成其重要的中间体3,5-二苯基溴苯,经过锂卤交换,采用还原蒽醌与相应芳基锂的加成物得到目标产物.研究了用所合成的材料作发光层所制得有机电致发光器件的光谱特性及其电流、电压、亮度等.结果表明通过改进的方法合成上述蓝色荧光材料具有原料易得、反应步骤少、产物得率较高等特点.

参考文献

[1] Tang C W,VanSlyke S A.Organic electroluminescent diodes[J].Appl.Phys.Lett.,1987,51(12):913-915.
[2] Tang C W,VanSlyke S A,Chen C H.Electroluminescence of doped organic thin films[J].J.Appl.Phys.,1989,65(9):3610-3616.
[3] Burroughes J H,Bradley D D C,Brown A R,et al.Light-emitting diodes based on conjugated polymers[J].Nature,1990,347(11):539-541.
[4] Hung L S,Tang C W,Mason M G.Enhanced electron injection in organic electroluminescence devices using an Al/LiF electrode[J].Appl.Phys.Lett.,1997,70(2):152-154.
[5] Baldo M A,O'Brien D F,You Y,et al.Highly efficient phosphorescent emission from organic electroluminescent devices[J].Nature,1998,395(6698):151-154.
[6] Kim Y H,Shin D C,Kim S H,et al.Novel blue emitting material with high color purity[J].Adv.Mater.,2001,13(22):1690-1693.
[7] Shi J M,Tang C W.Anthracene derivatives for stable blue-emitting organic electroluminescence devices[J].Appl.Phys.Lett.,2002,80(17):3201-3203.
[8] Kan Y,Wang L D,Duan L,et al.Highly-efficient blue electroluminescence based on two Emitter isomers[J].Appl.Phys.Lett.,2004,84(9):1513-1515.
[9] Shi J,Chen C H,Klubek K P.Organic electroluminescent elements for stable blue electroluminescent devices:US 5972247[P].1999-10-26.
[10] Jiang X Y,Zhang Z L,Zhang B X,et al.Stable blue and white organic light emitting diodes[J].Chin.J.Lumin.,2000,21(4):369-372.
[11] Miyaura N,Suzuki A.Palladium-Catalyzed cross-coupling reactions of organoboron compounds[J].Chem.Rev.,1995,95(7):2457-2483
[12] Wang W,Yang L,Zhang W,et al.Preparation of 5′-nitro-m-terphenyl and 5′-amino-m-terphenyl by Suzuki coupling reaction[J].Chemical Reagents,1999,21(1):51.
[13] Kelly T R,Chandrakumar N S,Saha J K.Achiral catechol with C2 symmetry[J].J.Org.Chem.,1989,54(4):980-983.
[14] Hodgson H H,Mahadevan A P.A interpretation of sandmeyer reaction(Part IX)[J].J.Chem.Soc.,1947:173-174.
[15] Du C-J Frank,Hart H,Ng K-K Daniel.A one-pot synthesis of m-terphenyls via a two-aryne sequence[J].J.Org.Chem.,1986,51(16):3162-3165.
[16] Ware W R,Rothman W.Relative fluorescence quantum yields using an integrating sphere.The quantum yield of 9,10-diphenylanthracene in cyclohexane[J].Chem.Phys.Lett.,1976,39(3):449-453.
上一张 下一张
上一张 下一张
计量
  • 下载量()
  • 访问量()
文章评分
  • 您的评分:
  • 1
    0%
  • 2
    0%
  • 3
    0%
  • 4
    0%
  • 5
    0%