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探索了纯石墨电极在水中放电制备洋葱状富勒烯(Onion-like fullerenes,OLFs)的过程和工艺.用高分辨透射电镜(High resolution transmission electron microscope,HRTEM)对生成的OLFs进行了形貌、结构的观察与表征.分析结果表明制得的OLFs具有各种不同形状的内核,石墨化程度很高,直径分布在5 nm~40 nm范围内.在一定范围内随着电流强度的增大OLFs的产量和产率都有不同程度的提高.

参考文献

[1] Iijima S .Helical microtubles of graphitic carbon[J].Nature,1991,354:56-58.
[2] Ugarte D .Curling and closure of graphitic networks under electron beam irradiation[J].Nature,1992,359:707-708.
[3] B.S.Xu;S.-I.Tanaka .Formation of giant onion-like fullerenes under Al nanoparticles by electron irradiation[J].Acta materialia,1998(15):5249-5257.
[4] Yuki Kimura;Takeshi Sato;Chihiro Kaito .Production and structural characterization of carbon soot with narrow UV absorption feature[J].Carbon: An International Journal Sponsored by the American Carbon Society,2004(1):33-38.
[5] Han PD;Xu BS;Jian L;Liu XG;Bao HQ .Band gaps of two-dimensional photonic crystal structure using fullerene films[J].Physica, E. Low-dimensional systems & nanostructures,2004(1):29-34.
[6] 章海霞,王晓敏,王海英,刘旭光,许并社.电弧法制备洋葱状富勒烯的工艺研究[J].新型炭材料,2004(01):61-64.
[7] N.I. Alekseyev;G.A. Dyuzhev .Fullerene formation in an arc discharge[J].Carbon: An International Journal Sponsored by the American Carbon Society,2003(7):1343-1348.
[8] Xu B S;Tanaka S I.Multiple nuclei onion like fullerenes cultivated by electron beam irradiation[M].Cambridge,1997:355-359.
[9] 闫小琴,张瑞珍,卫英慧,市野濑英喜,许并社.富勒烯制备方法研究的进展[J].新型炭材料,2000(03):63-69.
[10] Satoshi Tomita;Andrzej Burian;John C.Dore;David LeBolloch;Minoru Fujii;Shinji Hayashi .Diamond nanoparticles to carbon onions transformation: x-ray diffraction studies[J].Carbon: An International Journal Sponsored by the American Carbon Society,2002(9):1469-1474.
[11] Hiroaki Abe .Nucleation of carbon onions and nanocapsules under ion implantation at high temperature[J].Diamond and Related Materials,2001(3-7):1201-1204.
[12] 李天保,许并社,韩培德,张艳,王晓敏,刘旭光,市野濑英喜.洋葱状富勒烯的CCVD法制备及其形貌特征[J].新型炭材料,2005(01):23-27.
[13] Beck M T;Dinya Z;Keki S et al.Formation of C60 polycyclic aromatic hydrocarbons upon electric discharges in liquid toluene[J].Tetrahedron,1993,49:285-290.
[14] Su-Yuan Xie;Rong-Bin Huang;Li-Hua Chen;Wei-Jie Huang;Lan-Sun Zheng .Glow discharge synthesis and molecular structures of perchlorofluoranthene and other perchlorinated fragments of buckminsterfullerene[J].Chemical communications,1998(16):2045-2046.
[15] Ishigami M.;Zettl A.;Chen S.;Cumings J. .A simple method for the continuous production of carbon nanotubes[J].Chemical Physics Letters,2000(5-6):457-459.
[16] Sundaresan R;Bockris J O M .Anomalous reactions during arcing between carbon rods in water[J].Fusion technology,1994,26:261-265.
[17] Hsin YL.;Chen FR.;Kai JJ.;Hwang KC. .Production and in-situ metal filling of carbon nanotubes in water[J].Advanced Materials,2001(11):830-833.
[18] Zhu HW.;Li XS.;Jiang B.;Xu CL.;Zhu YF.;Wu DH.;Chen XH. .Formation of carbon nanotubes in water by the electric-arc technique[J].Chemical Physics Letters,2002(5-6):664-669.
[19] Sano N;Wang H;Alexandrou I et al.Synthesis of carbon onions' in water[J].Nature,2001,414:506-507.
[20] Kiselev NA.;Zakharov DN.;Kukovitskii EF.;Hutchison JL. Hammer J.;Kotosonov AS.;Sloan J. .Carbon nanotubes from polyethylene precursors: Structure and structural changes caused by thermal and chemical treatment revealed by HREM[J].Carbon: An International Journal Sponsored by the American Carbon Society,1998(7/8):1149-1157.
[21] 卢怡,朱珍平,刘振宇.催化剂对爆炸法合成碳纳米管的影响[J].新型炭材料,2004(01):1-6.
[22] 王晓敏,许并社,刘旭光,市野濑英喜.纳米金属微粒催化制备的洋葱状富勒烯的结构表征[J].新型炭材料,2004(03):209-213.
[23] 解思深,孙连峰.与富勒烯C36直径(0.5nm)相等的碳纳米管及其制备[J].物理,2000(10):577-578.
[24] N. Sano;H. Wang;I. Alexandrou;M. Chhowalla;K. B. K. Teo;G. A. J. Amaratunga;K. Iimura .Properties of carbon onions produced by an arc discharge in water[J].Journal of Applied Physics,2002(5):2783-2788.
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