采用原位水热合成法.分别采用四丙基氢氧化铵(TPAOH)和四丙基溴化铵(TPABr)为模板剂,在不锈钢片上合成出了6轴定向的siIicalite-1沸石膜.采用x射线衍射(XRD)和扫描电镜(SEM)对膜的定向性和晶体形貌进行表征.通过XRD和SEM图可以看出,合成出的沸石膜为连续的,且定向性较好.比较采用两种模板剂所合成出的沸石膜可以看出,采用四丙基氢氧化铵(TPAOH)合成出的沸石膜比采用四丙基溴化铵(TPABr)合成出的沸石膜定向性好,成膜速度较快,但晶体尺寸较小.
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