利用HRTEM和TEM研究了Al-Zn-Mg合金高能喷丸表面纳米化过程中微观结构的演变.结果表明,经表面高能喷丸处理,样品表面形成了厚度约20μm的纳米晶层,随温度的增加,平均晶粒尺寸由约20nm逐渐增加到约100nm;随着塑性变形量的增加,η′相在纳米晶区内几乎完全返溶,形成晶粒尺寸小于100nm的单相α过饱和固溶体.其原因可能是由于α固溶体的晶粒尺寸超细化而导致固溶度增加.
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