以溶胶、无定形及晶态的TiO2为原料,在合适的温度和氢氧化钠浓度下,水热合成了直径1~2 nm的钛酸钠盐纳米晶须和孔径~3.5 nm的纳米管.用XRD、TEM、N2吸附-脱附法分别表征了产物的组成、形貌和孔结构.以不同TiO2原料,控制反应液中有机杂质的含量,可得到晶须、纳米管或两者的混合物.
参考文献
[1] | Liu Z;Li Y X et al.[J].J Cera Soc,1998,26(03) |
[2] | Wu M Q;Chen A;Zhou W .[J].Chin J Cera Soc,2001,29(06) |
[3] | Kasuga T;Hiramatsu M et al.[J].Advanced Materials,1999,11:15. |
[4] | Zhang S L;Zhou J F;Zhang Z J;A V Vorontsov,Jin,Z S .[J].Chin Soc Bul,2000,45(10) |
[5] | Li Y D;Sun X M .[P].CN 02117866.6,2002. |
[6] | Zhang Q H;Gao L;Zheng S .[J].Acta Chem Sin,2002,60(08) |
[7] | Li W;Wang X D;Yang J J .[J].Journal of Chemical Research,2002,13(03) |
[8] | Wang Y Q;Hu G Q;Duan X F.[J].Chemical Physics Letters,2002:365. |
[9] | Song X C;Yue L H;Liu B .[J].Chinese Journal of Inorganic Chemistry,2003,19(08) |
[10] | Sun X M;Li Y D.[J].J Chem Eur,2003(09) |
[11] | Fu M;Jiang Z D;Ma Z F .[J].Journal of Inorganic Materials,2005,20(04) |
[12] | Xing Wu;Qi-Zhong Jiang;Zi-Feng Ma;Min Fu;Wen-Feng Shangguan .Synthesis of titania nanotubes by microwave irradiation[J].Solid State Communications,2005(9/10):513-517. |
[13] | Zhu H Y;Lan Y;Gao X P et al.[J].Journal of the American Chemical Society,2005,127:18. |
[14] | B Poudel;Wang W Z et al.[J].Nanotechnology,2005,16(09) |
[15] | Lan Y;Gao X P;Zhu H Y et al.[J].Advanced Functional Materials,2005,15(08) |
[16] | Yao B D;Chan Y F;Zhang X Y .[J].Apphed Physics Letters,2003,82(02) |
上一张
下一张
上一张
下一张
计量
- 下载量()
- 访问量()
文章评分
- 您的评分:
-
10%
-
20%
-
30%
-
40%
-
50%