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采用硬脂酸法在相对较低的温度下掺杂Nb制备了K2La1.8Nb0.2Ti3O10层状化合物.通过X射线衍射、透射电子显微镜、紫外-可见吸收光谱、拉曼光谱对产物进行了表征.结果表明,通过硬脂酸法在800℃可获得超细K2La1.8Nb0.2Ti3O10,颗粒尺寸为100~250 nm,经过Nb掺杂后的产物仍然保持层状结构,层间距约1.5nm.紫外-可见光谱表明掺杂前后的产物在紫外区均有较明显的吸收,但经Nb掺杂后的K2La1.8Nb0.2Ti3O10吸光度明显增强.

参考文献

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