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以β-环糊精(β-CD)、硝酸铋、溴化钾为原料,采用溶剂热法合成了银耳状BiOBr.通过X射线衍射(XRD)、扫描电镜(SEM)和紫外可见光谱(UV-Vis)对BiOBr粒子进行表征.实验发现:BiOBr的微观形貌与β-CD的用量有关,当β-CD的用量为0.4574 g时,所制得的BiOBr为银耳状,且其光催化性能最好.

参考文献

[1] Fujishima A;Honda K .Electrochemical photolysis of water at a semiconductor electrode[J].NATURE,1972,238:37.
[2] Thompson T L;Yates Jr J T .Surface science studies of the photoactivation of TiO2-new photochemical process[J].Chemical Reviews,2006,106:4428.
[3] 李海燕,钱俊杰,刘金凤,李秋叶,张敏,杨建军.氮铋共掺杂TiO2的合成及其可见光催化性能研究[J].影像科学与光化学,2013(06):411-420.
[4] 杨帆,李中和,蒋政.环境友好的BiOBr新型光催化剂制备、表征及其性能研究[J].洁净煤技术,2008(06):47-48,76.
[5] Huang, WL;Zhu, QS .Structural and electronic properties of BiOX (X = F, Cl, Br, I) considering Bi 5f states[J].Computational Materials Science,2009(4):1076-1084.
[6] Jiang Z;Yang F;Yang G D;Kong L Martin O J Xiao T C Edwards P P .The hydrothermal synthesis of BiOBr flakes for visible-light-responsive photocatalytic degradation of methyl orange[J].Journal of Photochemistry Photobiology A,2010,212:8-13.
[7] Kong, L.;Jiang, Z.;Xiao, T.;Lu, L.;Jones, M.O.;Edwards, P.P. .Exceptional visible-light-driven photocatalytic activity over BiOBr-ZnFe_2O_4 heterojunctions[J].Chemical communications,2011(19):5512-5514.
[8] Guohua Jiang;Xiaohong Wang;Zhen Wei .Photocatalytic properties of hierarchical structures based on Fe-doped BiOBr hollow microspheres[J].Journal of Materials Chemistry, A. Materials for energy and sustainability,2013(7):2406-2410.
[9] Zhang J;Shi FJ;Lin J;Chen DF;Gao JM;Huang ZX;Ding XX;Tang CC .Self-assembled 3-D architectures of BiOBr as a visible light-driven photocatalyst[J].Chemistry of Materials: A Publication of the American Chemistry Society,2008(9):2937-2941.
[10] Zhang X;Ai ZH;Jia FL;Zhang LZ .Generalized one-pot synthesis, characterization, and photocatalytic activity of hierarchical BiOX (X = Cl, Br, I) nanoplate microspheres[J].The journal of physical chemistry, C. Nanomaterials and interfaces,2008(3):747-753.
[11] Chen Y J;Wen M;Wu Q S .Stepwise blossoming of BiOBr nanoplate-assembled microflowers and their visible-light photocatalytic activities[J].CRYSTENGCOMM,2011,13:3035-3039.
[12] Hong Liu;Yun Su;Zhen Chen;Zhitong Jin;Yong Wang .Graphene sheets grafted three-dimensional BiOBr_(0.2)I_(0.8) microspheres with excellent photocatalytic activity under visible light[J].Journal of hazardous materials,2014(Feb.15):75-83.
[13] Jian Xu;Wei Meng;Yuan Zhang .Photocatalytic degradation of tetrabromobisphenol A by mesoporous BiOBr: Efficacy, products and pathway[J].Applied Catalysis, B. Environmental: An International Journal Devoted to Catalytic Science and Its Applications,2011(3/4):355-362.
[14] Lufeng Lu;Liang Kong;Zheng Jiang .Visible-Light-Driven Photodegradation of Rhodamine B on Ag-Modified BiOBr[J].Catalysis Letters,2012(6):771-778.
[15] Henle J;Simon P;Frenzel A;Scholz S;Kaskel S .Nanosized BiOX (X = Cl, Br, I) particles synthesized in reverse microemulsions[J].Chemistry of Materials: A Publication of the American Chemistry Society,2007(3):366-373.
[16] ZhangSheng Liu;BianTao Wu;DongHu Xiang;YaBo Zhu .Effect of solvents on morphology and photocatalytic activity of BiOBr synthesized by solvothermal method[J].Materials Research Bulletin: An International Journal Reporting Research on Crystal Growth and Materials Preparation and Characterization,2012(11):3753-3757.
[17] 肖培培 .溴氧化铋和硒碲化合物纳米材料的可控合成和表征[D].合肥:中国科学技术大学,2011.
[18] Yongli Li;Yuanming Liu;Jinshu Wang .Titanium alkoxide induced BiOBr-Bi2WO6 mesoporous nanosheet composites with much enhanced photocatalytic activity[J].Journal of Materials Chemistry, A. Materials for energy and sustainability,2013(27):7949-7956.
[19] Xuelei Wang;Jun Yang;Yuanyuan Chen;Yuanming Zhang;Yu Tang .EDTA-modified hydrothermal synthesis of a novel four-leaf clover-shape BiOBr microstructure[J].Materials Letters,2014(Feb.1):171-174.
[20] 贾志方 .新型可见光催化剂的制备及其光催化性能的研究[D].天津大学,2011.
[21] 魏平玉,杨青林,郭林.卤氧化铋化合物光催化剂[J].化学进展,2009(09):1734-1741.
[22] Wang X;Brusseau M L .Enhanced transport of low-polarity organic compounds through soil by cyclodextrin[J].Environmental Science and Technology,1993,27(12):2821-2825.
[23] Jiahui Zhang;Lili Zhang;jinshun Lv;Shouyong Zhou;Haiqun Chen;Yijiang Zhao;Xin Wang .Exceptional visible-light-induced photocatalytic activity of attapulgite-BiOBr-TiO_2 nanocomposites[J].Applied clay science,2014(Mar.):135-140.
[24] Jie Fu;Yanlong Tian;Binbin Chang .BiOBr-carbon nitride heterojunctions: synthesis, enhanced activity and photocatalytic mechanism[J].Journal of Materials Chemistry: An Interdisciplinary Journal dealing with Synthesis, Structures, Properties and Applications of Materials, Particulary Those Associated with Advanced Technology,2012(39):21159-21166.
[25] Kijima N;Matano K;Saito M;Oikawa T Konishi T Yasuda H Sato T Yoshimura Y J .Oxidative catalytic crack ing of n-butane to lower alkenes over layered BiOCl catalyst[J].Applied Catalysis A:General,2000,206:237-242.
[26] Wang J W;Li Y D .Synthesis of single-crystalline nanob clts of ternary bismuth oxide bromide with different compositions[J].Chemical Communications,2003,18:2320-2321.
[27] Sun X H;Zheng C M;Zhang F X;Li L D Yang Y L Wu G J Guan N J .β-Cyclodextrin-assisted synthesis of superparamagetic magnetite nanoparticles form a single Fe(Ⅲ) precursor[J].Journal of Physical Chemistry C,2008,112(44):17148-17155.
[28] Yu L;Xue W H;Cui L;Xin W Cao X L Li H Y .Use of hydroxypropyl-β-cyclodextrin/ polyethylene glycol 400,modified Fe3O4 nanoparticles for congo red removal[J].International Journal of Biological Macromolecules,2014,64:233-239.
[29] Bin Zhao;Huilan Chen .Synthesis novel multi-petals ZnO nano-structure by a cyclodextrin assisted solution route[J].Materials Letters,2007(27):4890-4893.
[30] 赵雯雯,刘亚威,张昌远,黄祥平,毛峰,杨学林.醇热法BiOCl微米球的制备及其性能研究[J].三峡大学学报(自然科学版),2011(06):106-109.
[31] AN Huizhong,DU Yi,WANG Tianmin,WANG Cong,HAO Weichang,ZHANG Junying.Photocatalytic properties of BiOX (X=Cl, Br, and I)[J].稀有金属(英文版),2008(03):243-250.
[32] Xia, J.;Yin, S.;Li, H.;Xu, H.;Xu, L.;Xu, Y. .Improved visible light photocatalytic activity of sphere-like BiOBr hollow and porous structures synthesized via a reactable ionic liquid[J].Dalton transactions: An international journal of inorganic chemistry,2011(19):5249-5258.
[33] Batabyal S K;Basu C;Sanyal G S;Das A R .Synthesis of Sb2Se3 nanorod using β-cyclodextrin[J].Materials Letters,2003,58(01):169-171.
[34] 秦帆,吴际良,吕中,余响林,陈嵘.微波法合成硫化铋纳米棒[J].北京科技大学学报,2010(05):638-643.
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