为研究稀土锆酸盐热障涂层的抗热震性能及隔热性能,以Sm2O3和ZrO2为原料,采用固相反应法制备了热喷涂用Sm2Zr2O7粉末,并采用大气等离子喷涂技术在LY12合金表面制备了Sm2Zr2O7热障涂层.利用X射线衍射(XRD)、扫描电镜(SEM)等测试技术研究了Sm2Zr2O7粉末和Sm2Zr2O7涂层的微观组织结构、涂层结合强度和热导率.结果表明:制备的Sm2Zr2O7粉末主要呈短轴状,颗粒内部结合紧密,可满足热喷涂的需要;喷涂前后Sm2Zr2O7相成分没有发生任何变化,具有良好的相稳定性能;Sm2Zr2O7热障涂层组织结构致密,涂层的孔隙率约为14.31%,结合强度约为19.8 MPa;在相同的孔隙率下,Sm2Zr2O7涂层的热导率仅为YSZ涂层的37.6%和纳米YSz涂层的42.1%.
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