利用微波进行化学合成是近年发展起来的一种简单、快捷、高效的合成方法.综述了微波在有序介孔材料合成、模板剂脱除和在介孔材料负载活性组分中的应用,介绍了一些典型的有序介孔材料的微波合成新进展,指出了该方法在有序介孔材料合成中的优势及发展前景.
参考文献
| [1] | Jun S.;Ryoo R.;Kruk M.;Jaroniec M.;Liu Z.;Ohsuna T. Terasaki O.;Joo SH. .Synthesis of new, nanoporous carbon with hexagonally ordered mesostructure[J].Journal of the American Chemical Society,2000(43):10712-10713. |
| [2] | Rao, KJ;Ganguli, M;Ramakrishnan, PA;Vaidhyanathan, B .Synthesis of inorganic solids using microwaves[J].Chemistry of Materials,1999(4):882-895. |
| [3] | Liang JH.;Deng ZX.;Jiang X.;Li FL.;Li YD. .Photoluminescence of tetragonal ZrO2 nanoparticles synthesized by microwave irradiation[J].Inorganic Chemistry: A Research Journal that Includes Bioinorganic, Catalytic, Organometallic, Solid-State, and Synthetic Chemistry and Reaction Dynamics,2002(14):3602-3604. |
| [4] | oxallDL;Lukehart C M .Rapid synthesisof Ptor Pd/Carbon nanocomposites using microwave irradiation[J].CHEMISTRY OF MATERIALS,13:806. |
| [5] | HanYu;Ma Hao;Qiu Shilin et al.Preparation of zeolite A membranes by microwave heating[J].Microporous and Mesoporous Materials,1999,30:321. |
| [6] | HuangLimin;Wang Zhengbao;Wang Huanting et al.Hierarchical porous structures by using zeolite nanocrystals as building blocks[J].Microporous and Mesoporous Materials,2001,48:73. |
| [7] | XuXiaochun;Yang Weishen;Liu Jie et al.Synthesis of NaA zeolite membrane by microwave heating[J].Separation and Purification Technology,2001,25:241. |
| [8] | GirnusI;Jancke K;Vetter R .Large AlPO4-5 crystals by microwave heating[J].Zeolites,1995,15:33. |
| [9] | KodairaTetsuya;Miyazawa Kohji;Ikeda Takuji et al.Synthesis of AlPO4-5 powder by microwave heating: Influence of starting gel pH and reaction time[J].Microporous and Mesoporous Materials,1999,29:329. |
| [10] | KuniiKatsuyuki;Narahara Kazuhiro;Yamanaka Shoji .Template-free synthesis of A1PO4-H1, -H2, and-H3 by microwave heating[J].Microporous and Mesoporous Materials,2002,52:159. |
| [11] | TuW;Liu H .Continuous synthesis of colloidal metal nanoclusters by microwave irradiation[M].Chem Mater,2000,12:564. |
| [12] | KresgeCT;Leonowicz M E;Roth W J .Ordered mesoporous molecular sieves synthesized by a liquid-crystal template mechanism[J].Nature,1992,359:710. |
| [13] | WuCG;Bein T.Microwave synthesis of molecular sieve MCM-41[J].Chemical Communications,1996:925. |
| [14] | ParkSE;Kim D S;Chang J S .Synthesis of MCM-41 using microwave heating with ethylene glycol[J].Catalysis Today,1998,44:301. |
| [15] | 许磊,王公慰,魏迎旭,齐越,刘宪春,包信和.MCM-41介孔分子筛合成研究Ⅱ.微波辐射合成法[J].催化学报,1999(03):251-255. |
| [16] | 姚云峰,张迈生,杨燕生.纳米介孔分子筛MCM-41的微波辐射合成法[J].物理化学学报,2001(12):1117-1121. |
| [17] | 张青山,张辉淼,郭炳南.以双子表面活性剂为模板全微波辐射合成介孔分子筛MCM-48[J].北京理工大学学报,2003(03):394-396. |
| [18] | Zhao DY.;Feng JL.;Chmelka BF.;Stucky GD.;Huo QS. .Nonionic triblock and star diblock copolymer and oligomeric surfactant syntheses of highly ordered, hydrothermally stable, mesoporous silica structures[J].Journal of the American Chemical Society,1998(24):6024-6036. |
| [19] | NewalkarharatL;Komarneni Sridhar et al.Rapid synthesis of mesoporous SBA-15 molecular sieve by a microwave-hydrothermal process[J].Chemical Communications,2000,23:2389. |
| [20] | NewalkarL;Komarneni S .Simplified synthesis of micropore-free mesoporous silica, SBA-15, under microwave-hydrothermal conditions[J].Chemical Communications,2002,16:1774. |
| [21] | NewalkarL;Komarneni S.Control over microporosity of ordered microporous-mesoporous silica SBA-15 framework under microwave-hydrothermal conditions: effect of salt addition[M].Chem Mater,2001:4573. |
| [22] | Newalkar BL.;Komarneni S.;Turaga UT.;Katsuki H. .Synthesis and characterization of PSU-1, a novel cage-like mesoporous silica[J].Journal of Materials Chemistry: An Interdisciplinary Journal dealing with Synthesis, Structures, Properties and Applications of Materials, Particulary Those Associated with Advanced Technology,2003(7):1710-1716. |
| [23] | He J.;Yang XB.;Evans DG.;Duan X. .New methods to remove organic templates from porous materials[J].Materials Chemistry and Physics,2003(1):270-275. |
| [24] | Tianozhi;Liu Xiaoying;Zhao Dongyuan et al.Microwave assisted template removal of siliceous porous materials[J].Chemical Communications,2002,11:1186. |
| [25] | LangNatacha;Deliehere Pierre;Tuel Alain .Post-synthesis introduction of transition metals in surfactant-containing MCM-41 materials[J].Microporous and Mesoporous Materials,2002,56:203. |
| [26] | ourlinosA;Karakassides M A;Petridis D .Synthesis and characterization of iron-containing MCM-41 porous silica by the exchange method of the template[J].Journal of Physical Chemistry B,2000,2000(104):4375. |
| [27] | LuanZ;Bae J Y;Kevan L .Vanadosilicate mesoporous SBA-15 molecular sieves incorporated with N-Alkylphenothiazines[J].Chemistry of Materials,2000,12(10):3202. |
| [28] | Zhang WH.;Lu JQ.;Han B.;Li MJ.;Xiu JH.;Ying PL.;Li C. .Direct synthesis and characterization of titanium-substituted mesoporous molecular sieve SBA-15[J].Chemistry of Materials,2002(8):3413-3421. |
| [29] | Anagha Belhekar;Mangala Agashe;Hirji Soni;Shivaram Sathaye;Nalini Jacob;Jyothi Thundimadathil .Synthesis and Characterization of Titanium-Containing Mesoporous Silica by a Non-Hydrothermal Microwave Method[J].Bulletin of the Chemical Society of Japan,2000(11):2605-2608. |
| [30] | Kyoung-KuKang;Chan-Ho Park;Wha-Seung Ahn .Microwave preparation of a titanium-substituted mesoporous molecular sieve[J].Catalysis Letters,1999,59:45. |
| [31] | 赵杉林,张扬建,孙桂大,翟玉春.钛硅沸石分子筛TiMCM-41的微波合成与表征[J].催化学报,1999(01):93-95. |
| [32] | 赵杉林,张扬健,孙桂大,翟玉春.钒硅MCM-41沸石分子筛微波合成与表征[J].燃料化学学报,1999(02):130-133. |
| [33] | 张扬健,赵杉林,孙桂大,王振龙.W-MCM-48中孔分子筛的微波合成与表征[J].催化学报,2000(04):345-349. |
| [34] | NewalkarL;Olanrewaju J;Komarneni S.Direct synthesis of titanium-substituted mesoporous SBA-15 molecular sieve under microwave-hydrothermal conditions[M].Chem Mater,2001:552. |
| [35] | NewalkarL;Olanrewaju J;Komarneni S .Microwavehydrothermal synthesis and characterization of zirconium substituted SBA-15 mesoporous silica[J].Journal of Physical Chemistry B,2001,105:8356. |
| [36] | 颜学武,韩小伟,曹毅,魏一伦,朱建华.微波法研制碱土金属氧化物负载型MCM-48碱性介孔材料[J].无机化学学报,2002(11):1101-1106. |
| [37] | 魏一伦,曹毅,朱建华,颜学武.MgO/SBA-15固体碱介孔材料的研制[J].无机化学学报,2003(03):233-239. |
| [38] | YaoYunfeng;Zhang Maisheng;Shi Jianxin et al.Encapsulation of fluorescein into MCM-41 mesoporous molecular sieve by a sol-gel method[J].Materials Letters,2001,48:44. |
| [39] | ZhangGuangyu;Jiang Xin;Wang Enge .Tubular graphite cones[J].Science,2003,300:47. |
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