通过对热连轧(HCR)GH4169合金进行不同工艺热处理、蠕变性能测试和组织形貌观察,研究了热处理工艺对HCR合金组织与蠕变性能的影响。结果表明:热连轧合金中晶粒细小,具有明显的孪晶特征;HCR合金经直接时效后,大量细小γ"相在晶内弥散析出,可提高合金的蠕变抗力,在660℃、700 MPa条件下,使合金的蠕变寿命由60 h提高到126 h;经长期时效处理后,合金中的晶粒尺寸和γ"相略有长大,同时有NbC、Cr7C3碳化物在晶内析出。在蠕变过程中,HCR合金的变形特征是孪晶变形及孪晶内发生位错的双取向滑移;DA合金与LTA合金具有相近的蠕变寿命,其变形特征仍然是孪晶变形和晶内的位错滑移。
Influences of heat treatment on microstructure and creep properties of hot-continuous-rolled(HCR) GH4169 superalloy were investigated by means of creep tests,SEM and TEM.Results show that smaller grain size and twinning feature are displayed in the HCR alloy.After direct aging(DA),a large amount of fine γ" phase dispersively distributed in the alloy is observed,which improves creep resistance of the alloy and enhances creep lifetime from 60 h to 126 h under applied stress of 700 MPa at 660 ℃.After long term aging(LTA) treatment,the size of the grain and γ" phase in the alloy increases slightly,and NbC,Cr7C3 carbides are precipitated within grains of the alloy.The deformation of the HCR alloy during creep is characterized by twinning and double orientations slipping of dislocations.The DA and LTA alloys exhibit similar creep resistance,and the creep deformation mechanism of twinning and slipping of dislocations within grains is observed for the DA and LTA alloy.
参考文献
[1] | 王岩,林琳,邵文柱,甄良,张新梅.固溶处理对GH4169合金组织与性能的影响[J].材料热处理学报,2007(z1):176-179. |
[2] | M. Nageswara Rao .Factors influencing the notch rupture life of superalloy 718[J].Transactions of the Indian Institute of Metals,2010(2/3):363-367. |
[3] | 曹美华,陈国胜,周奠华,庞克昌.变形速度及晶粒度对GH4169合金高温拉伸性能和组织的影响[J].钢铁研究学报,2003(z1):361-365. |
[4] | 李荣斌,姚枚,刘文昌,张伟红,何贤昶.直接时效工艺对INCONEL 718合金组织的影响[J].金属热处理,2002(02):21-22. |
[5] | Tian S G;Li Z R;Zhao Z G.Influece of direct aging treatment on creep behaviors of hot continuous rolled GH4169 superalloy[M].Warrendale,USA,TMS,2010:455-462. |
[6] | G. Appa Rao;Mahendra Kumara;M. Srinivas .Effect of standard heat treatment on the microstructure and mechanical properties of hot isostatically pressed superalloy inconel 718[J].Materials Science & Engineering, A. Structural Materials: Properties, Misrostructure and Processing,2003(1/2):114-125. |
[7] | 宁永权,姚泽坤,郭鸿镇,田军强,虢迎光.等温锻造对IN718合金组织和性能的影响[J].热加工工艺,2007(21):65-67. |
[8] | 崔彤,王继杰,王磊,杨洪才,赵光普.长期时效对一种新型镍基合金的组织及持久性能的影响[J].材料热处理学报,2006(05):56-59. |
[9] | 肖素芬;陈梦谪;王宁 等.粉末718合金析出相长期时效的TEM探究[J].金属学报,1996,32(06):12-16. |
[10] | 陈国胜,王庆增,张玩良,李伟,王资兴,刘丰军,王世普.GH4169合金细晶棒材的连轧工艺及其组织与性能[J].材料工程,2010(04):18-21. |
[11] | Rao GA;Srinivas M;Sarma DS .Effect of thermomechanical working on the microstructure and mechanical properties of hot isostatically pressed superalloy Inconel 718[J].Materials Science & Engineering, A. Structural Materials: Properties, Misrostructure and Processing,2004(2):201-212. |
[12] | 郭士文,张玉锁,童开峰,杨洪才.镍基高温合金长期时效后γ′相长大动力学[J].东北大学学报(自然科学版),2003(06):576-579. |
[13] | 邓群;庄景云;杜金辉 等.GH169合金A高温长期时效后的组织性能变化[J].钢铁研究学报,1998,10(02):34-36. |
[14] | 孔永华,李龙,陈国胜,朱世根.不同热处理工艺对GH4169合金组织及性能的影响[J].稀有金属材料与工程,2010(z1):472-475. |
[15] | 谢锡善,董建新,付书红,张麦仓.γ"和γ'相强化的Ni-Fe基高温合金GH4169的研究与发展[J].金属学报,2010(11):1289-1302. |
- 下载量()
- 访问量()
- 您的评分:
-
10%
-
20%
-
30%
-
40%
-
50%