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以碳酸钙(CaCO3)为原料利用溶胶-凝胶法与热分解法合成了CaCO3纳米线,纳米线的制备分为两个步骤,首先利用溶胶-凝胶法合成线状含Ca中间体,这种含Ca中间体是一维线状纳米结构;然后通过含Ca中间体热分解制得CaCO3纳米线,直径为50-80nm,长度达5μm以上,所得CaCO3纳米线为三方晶系,由纳米晶粒组装而成.

CaCO3 nanowires were synthesized from CaCO3 reagent by sol-gel process and thermal decomposition. The preparation of CaCO3 included two steps: In the first step, the wirelike intermediates containing Ca were synthesized by sol-gel process, which are with one dimension wire-like nanostructures; in the second step, the resulting samples were converted into CaCO3 nanowires by thermal decomposition. The diameter and length of the obtained nanowires are 50-80nm and up to 5μm separately. The nanowires are constited of self-assembled nanoparticles and they belong to the trigonal system.

参考文献

[1] Wang Zhenghua, Chen Xiangying. Chem. Lett., 2004, 33(6): 754-755.
[2] Sun Chunwen, Li Hong, Wang ZhaoXiang. Chem. Lett., 2003, 33(6): 662-663.
[3] Wang Zhonglin. J. Phys: Condens. Matter., 2004, 16(25): R829-R858.
[4] Zheng Nengwu, Wu Qingsheng, Ding Yaping. Chem. Lett., 2000, 33(6): 638-639.
[5] Qi Limin, Ma Jiming, Cheng Humin. J. Phys. Chem. B, 1997, 101(18): 3460-3463.
[6] 高远浩, 牛和林, 陈乾旺. 无机化学学报, 2003, 19(1): 37-40.
[7] Yu Shu-Hong, Markus Antonietti, Helmut Colfen. Nano Lett., 2003, 3(3): 379-382.
[8] 高远浩, 李灵芝, 牛和林. 化学通报, 2004, 67(5): 383-386.
[9] Tsay Jenq-dar, Fang Tsang-tse. J. Am. Ceram. Soc., 1999, 82(6): 1409-1415.
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