表面技术 , 2014, (3): 90-110.
曼尼希碱与硫脲在气井采出水腐蚀体系中的缓蚀协同作用
孟凡宁 1, , 李谦定 2, , 李善建 3, {"currentpage":1,"firstResult":0,"maxresult":10,"pagecode":5,"pageindex":{"endPagecode":5,"startPagecode":1},"records":[{"abstractinfo":"研究了不同含镍量的低合金钢在青岛和江津的大气腐蚀,结果表明,含镍量2.68%的合金钢在含硫、氯的环境下都有较好的抗腐蚀性能,抵抗氯对钢材侵蚀的效果比抵抗硫对钢材侵蚀的效果更显著.对锈层的X射线衍射定量相分析表明,含镍量2.68%的合金钢在青岛暴露24个月的锈层中的δ-FeOOH和α-FeOOH更多,β-FeOOH少,说明含镍钢在含氯的环境下更易形成致密锈层,阻碍Cl-的渗透.","authors":[{"authorName":"顾家琳","id":"57a9d70a-c68d-477c-8be0-750e01cf8ff8","originalAuthorName":"顾家琳"},{"authorName":"闫睿","id":"dd0612e9-6eee-4685-90d5-5212776e11a6","originalAuthorName":"闫睿"},{"authorName":"久本淳","id":"b5447400-b8be-4349-9e0a-32804b325f99","originalAuthorName":"久本淳"},{"authorName":"濑文雄","id":"8ecf9a2c-6418-4736-8799-4e24a6e0b035","originalAuthorName":"濑文雄"}],"doi":"","fpage":"5","id":"786ed38f-a42c-433e-8b4f-346b571ef991","issue":"1","journal":{"abbrevTitle":"FSYFH","coverImgSrc":"journal/img/cover/FSYFH.jpg","id":"25","issnPpub":"1005-748X","publisherId":"FSYFH","title":"腐蚀与防护"},"keywords":[{"id":"bdab4555-8dbd-4d64-a4ed-05013742237e","keyword":"镍","originalKeyword":"镍"},{"id":"d1b566fb-b428-411a-bc43-602d7b197a49","keyword":"大气腐蚀","originalKeyword":"大气腐蚀"},{"id":"3a8a8409-f76b-4e81-bd7c-8d02f548bddb","keyword":"硫","originalKeyword":"硫"},{"id":"44d233a4-e063-4d5f-8e3a-680c8214e6c4","keyword":"氯","originalKeyword":"氯"}],"language":"zh","publisherId":"fsyfh201001002","title":"镍含量对钢材大气腐蚀的影响","volume":"31","year":"2010"},{"abstractinfo":"研究碳钢在青岛不同暴露方式下的大气腐蚀,结果表明:带顶盖的腐蚀面向上的B种暴露方式和带顶盖腐蚀面向下的C种暴露方式要比面朝南且与水平倾斜45°的A种暴露方式的大气腐蚀严重得多.认为这种现象与青岛的高湿度及Cl-的影响有关.","authors":[{"authorName":"顾家琳","id":"f1de6f76-c889-4344-a0bb-5da89923884e","originalAuthorName":"顾家琳"},{"authorName":"闫睿","id":"3ac4a252-50dd-473d-b1d2-ee58c70f9f93","originalAuthorName":"闫睿"},{"authorName":"久本淳","id":"f4f9c270-c12b-40c3-8578-3db29d231424","originalAuthorName":"久本淳"},{"authorName":"濑文雄","id":"b20117aa-c71e-47d5-abb1-3290499984e7","originalAuthorName":"濑文雄"}],"doi":"10.3969/j.issn.1001-4381.2009.12.009","fpage":"37","id":"a4bd770a-dab3-45e7-83e3-d171bf817f31","issue":"12","journal":{"abbrevTitle":"CLGC","coverImgSrc":"journal/img/cover/CLGC.jpg","id":"9","issnPpub":"1001-4381","publisherId":"CLGC","title":"材料工程"},"keywords":[{"id":"e2404aa4-5c72-41b6-9b1c-6649421bbb1d","keyword":"碳钢","originalKeyword":"碳钢"},{"id":"8f98cdfe-3915-4308-b03a-179c45f25b46","keyword":"大气腐蚀","originalKeyword":"大气腐蚀"},{"id":"cf6de2e6-bd4c-4078-b4ca-95af7f5cf634","keyword":"暴露方式","originalKeyword":"暴露方式"}],"language":"zh","publisherId":"clgc200912009","title":"碳钢在青岛不同暴露方式下的大气腐蚀","volume":"","year":"2009"},{"abstractinfo":"以醋酸去氢表雄酮为起始原料,于温度为65～70℃的DMSO-甲苯混合溶剂中,反应时间为22 h,利用二碘酰基苯甲酸(IBX)对醋酸去氢表雄酮的选择性脱氢简便高效地合成了曲螺酮关键中间体3β-乙酰氧基-雄甾-△4,15-二烯-17-酮;探讨了IBX与醋酸去氢表雄酮的摩尔比对目标化合物的收率影响.实验表明.在n(IBX):n(醋酸去氢表雄酮)=1.5∶1.0时,目标化合物的收率最佳,达到73%.目标化合物经紫外光谱、红外光谱、核磁共振氢谱、质谱及元素分析测试技术确证了其化学结构.","authors":[{"authorName":"贺诗华","id":"10e09bce-0f1c-4da2-a46e-8f4a52ddc3d0","originalAuthorName":"贺诗华"},{"authorName":"WANG Chun-Ting","id":"bdce8fe1-6816-44fc-be7c-745d0561e9a4","originalAuthorName":"WANG Chun-Ting"}],"doi":"10.3969/j.issn.1000-0518.2008.08.028","fpage":"992","id":"7f557618-a2da-4590-9eaa-731450d12c72","issue":"8","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"443eb0f0-e283-49f5-9eee-85ef2b28b31f","keyword":"醋酸去氢表雄酮","originalKeyword":"醋酸去氢表雄酮"},{"id":"531409dd-8d3f-4e1d-a203-959cb2b26fe9","keyword":"IBX","originalKeyword":"IBX"},{"id":"d2f377e1-52cc-4022-b8d4-860fd9e5cfb1","keyword":"β-乙酰氧基-雄甾-△5","originalKeyword":"β-乙酰氧基-雄甾-△5"},{"id":"582d52ac-7d46-4c8e-8a6e-2b9faff38d29","keyword":"15-二烯.酮","originalKeyword":"15-二烯.酮"},{"id":"8e8795d5-a2d3-438c-bee5-ba81fc378b71","keyword":"αβ-不饱和羰基甾体","originalKeyword":"αβ-不饱和羰基甾体"},{"id":"b8d1f8c6-e9a5-4a8c-96f0-3982a60608c4","keyword":"中间体","originalKeyword":"中间体"}],"language":"zh","publisherId":"yyhx200808028","title":"用IBX对醋酸去氢表雄酮选择性脱氢合成3β-乙酰氧基-雄甾-△5,15-二烯-17-酮","volume":"25","year":"2008"},{"abstractinfo":"去氢表雄酮醋酸酯经过氧甲酸环氧化、高碘酸开环、IBX氧化、脱水和碱性水解等5步反应,以55%的总收率合成得到了非雄性激素芳香化酶抑制剂3β-羟基雄甾-4-烯-6,17-二酮.在环氧化反应中,利用价廉、易制备的过氧甲酸以几乎定量的收率得到了环氧化合物.使用IBX氧化邻二醇,以98.5%的收率得到氧化产物,避免了使用处理困难并且污染环境的铬试剂.","authors":[{"authorName":"江敏","id":"e478bfe0-208e-4d40-a891-eedb9cf14a31","originalAuthorName":"江敏"},{"authorName":"崔鹏","id":"91ed401e-c66f-41df-ba36-6f08c9699a8d","originalAuthorName":"崔鹏"},{"authorName":"于涛","id":"dffde2e4-50e3-4398-be98-215e1e3e278a","originalAuthorName":"于涛"},{"authorName":"杨帆","id":"e7bdeb82-e4d2-42bc-a46a-8613db59cac6","originalAuthorName":"杨帆"},{"authorName":"汤杰","id":"463f6e76-b476-41cd-bcf8-ec1e609dab13","originalAuthorName":"汤杰"}],"doi":"10.3969/j.issn.1000-0518.2006.12.028","fpage":"1422","id":"bb4b6099-3bef-4f3f-ae66-f1f81d5a1cf8","issue":"12","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"fb0499b0-9a73-4045-887b-8e6206996906","keyword":"3β-羟基雄甾烯二酮","originalKeyword":"3β-羟基雄甾烯二酮"},{"id":"736c2718-509a-4751-a5d8-3fd2eff0bb2d","keyword":"IBX","originalKeyword":"IBX"},{"id":"b13d7ec9-7e89-4df5-91fe-02c2a29babe6","keyword":"合成","originalKeyword":"合成"}],"language":"zh","publisherId":"yyhx200612028","title":"3β-羟基雄甾-4-烯-6,17-二酮的合成","volume":"23","year":"2006"},{"abstractinfo":"以去氢表雄酮(1)为原料,经过氯铬酸吡啶(PCC)氧化得到雄甾-4-烯-3,6,17-三酮(2),然后在Co2+存在下用NaBH4还原,得到芳香酶的强效抑制剂3β-羟基雄甾-4-烯-6,17-二酮(3). 与文献合成方法相比,反应步骤缩短,反应产率提高. 化合物3的结构经NMR和IR测试技术进行了表征,与文献结果一致.","authors":[{"authorName":"张晓佳","id":"a0e3f7d2-e402-4a37-aba8-0f80dc2d5b48","originalAuthorName":"张晓佳"},{"authorName":"崔建国","id":"768d7ce8-02b0-479c-97c6-e6cc70f98388","originalAuthorName":"崔建国"},{"authorName":"李莹","id":"f3549be9-434c-4b1f-a284-604430db6b60","originalAuthorName":"李莹"},{"authorName":"范建春","id":"1c6c993e-32db-4cd3-ba64-9301f4a7a512","originalAuthorName":"范建春"}],"doi":"10.3724/SP.J.1095.2010.90429","fpage":"615","id":"3e32b24d-4ae2-4cfc-95ac-0496eaea79c5","issue":"5","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"84cb8df9-fa7f-430f-af32-283b5de84ad7","keyword":"去氢表雄酮","originalKeyword":"去氢表雄酮"},{"id":"cf0aa859-4ca0-4f2b-a3fe-d0c278518532","keyword":"3β-羟基雄甾烯二酮","originalKeyword":"3β-羟基雄甾烯二酮"},{"id":"02f9c6df-2b66-4f6a-a31e-35af35ed0f98","keyword":"合成","originalKeyword":"合成"}],"language":"zh","publisherId":"yyhx201005024","title":"3β-羟基雄甾-4-烯-6,17-二酮合成的一种新方法","volume":"27","year":"2010"},{"abstractinfo":"采用对甲苯磺酸(pTsOH)和i氟乙酸(TFA)为催化剂,邻碘酰苯甲酸(IBX)为氧化剂,于40-45℃,在T01.DMSO混合溶剂中,将醋酸去氢表雄酮选择性脱氢,简便高效地制备了3β-乙酰氧基.雄甾-5.15-二烯-17-酮(I),产率分别为77%和89%.本合成线路有效避免了经溴代脱溴和发酵等合成线路反应繁多、试剂毒性大、成本高以及单纯IBX选择性脱氢反应温度高、反应时间长等不足.然后将化合物I在碱性条件下水解得到3β-羟基.雄甾-5,15-二烯-17-酮(Ⅱ),产率92%.最后将化合物Ⅱ与碘化三甲基氧化锍进行迈克尔共轭加成制得目的物15β,16β-亚甲基.雄甾-5-烯-3β-醇-17-酮(Ⅲ),产率89%.中间体和目的物经紫外光谱、红外光谱、核磁共振氧谱、质谱及元素分析确证了其化学结构.","authors":[{"authorName":"贺诗华","id":"2b14f0e0-fde8-4e8a-9ec8-d52a03a85213","originalAuthorName":"贺诗华"}],"doi":"10.3969/j.issn.1000-0518.2009.04.008","fpage":"405","id":"2fd086f4-7e54-4847-8967-f93367e2121b","issue":"4","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"77f7c9ee-7c9f-40c7-9f9e-5f80a26dc617","keyword":"醋酸去氢表雄酮","originalKeyword":"醋酸去氢表雄酮"},{"id":"ba4fe187-e69d-4cc2-86be-81d24c3bdb7d","keyword":"IBX","originalKeyword":"IBX"},{"id":"d51fa099-b86a-47b6-bbd4-db9f43e7b3ac","keyword":"15β","originalKeyword":"15β"},{"id":"cad463b9-5284-48e8-94a2-5186846f3d94","keyword":"16β-亚甲基-雄甾烯-3β-醇酮","originalKeyword":"16β-亚甲基-雄甾烯-3β-醇酮"},{"id":"4e882fea-712c-4dad-930f-fc8ee3da9e4e","keyword":"α","originalKeyword":"α"},{"id":"24e47773-c5a2-48d7-b1cf-9dfb73b19575","keyword":"β-不饱和羰基甾体","originalKeyword":"β-不饱和羰基甾体"},{"id":"d13311f5-a635-4804-a9cd-fb20816d58aa","keyword":"中间体","originalKeyword":"中间体"}],"language":"zh","publisherId":"yyhx200904008","title":"简便高效合成15β,16β-亚甲基-雄甾-5-烯-3β-醇-17-酮","volume":"26","year":"2009"},{"abstractinfo":"为了研究雄烯二酮（4?androstene?3，17?dione， AED）长期暴露对食蚊鱼（ Gambusia affinis）肝脏7?乙氧基?3?异酚恶唑脱乙基酶（EROD）和谷胱甘肽硫转移酶（GST）的影响，分别利用不同浓度的AED（0．14、1．4、14、140 nmol·L－1和420 nmol·L－1）对食蚊鱼仔鱼进行180 d的水浴暴露，同时设丙酮和空白对照组，分别于第180天取样后测定肝脏的EROD和GST活性．结果表明，与对照组相比，AED对食蚊鱼雌性幼鱼的体重和体长均起到显著的抑制作用，对食蚊鱼雄性幼鱼的体重和体长的影响不明显，只有最高浓度起抑制作用． AED对食蚊鱼幼鱼EROD的抑制作用与暴露浓度呈显著的剂量关系．各浓度组AED对雌性食蚊鱼幼鱼和雄性食蚊鱼幼鱼GST活性的影响大致呈现出倒“U”曲线的趋势．","authors":[{"authorName":"侯丽萍","id":"549aa620-a9ef-490d-9372-a44e300f810c","originalAuthorName":"侯丽萍"},{"authorName":"舒琥","id":"89bf4d65-419b-4ae6-b74a-23b70fc2584c","originalAuthorName":"舒琥"},{"authorName":"李海鹏","id":"f6e0f095-7b8d-4ae9-957e-26754c912720","originalAuthorName":"李海鹏"},{"authorName":"刘珊","id":"4d59d2ff-18e7-46a2-8a33-99d1f8b64b46","originalAuthorName":"刘珊"},{"authorName":"赵建亮","id":"f7778131-ba13-4661-b94c-8a2f03e90bec","originalAuthorName":"赵建亮"},{"authorName":"方展强","id":"63527615-0003-4124-b4dd-c4d57ebcff26","originalAuthorName":"方展强"}],"doi":"10.7524/j.issn.0254-6108.2015.03.2014071001","fpage":"442","id":"4c35572a-73ad-4a4a-b456-82af8d1bf983","issue":"3","journal":{"abbrevTitle":"HJHX","coverImgSrc":"journal/img/cover/HJHX.jpg","id":"43","issnPpub":"0254-6108","publisherId":"HJHX","title":"环境化学 "},"keywords":[{"id":"133d05d5-fea7-4d3e-802f-4f95f2791bfe","keyword":"雄烯二酮","originalKeyword":"雄烯二酮"},{"id":"f4a6f146-80a1-454f-9b9b-f70b84a52dc3","keyword":"食蚊鱼","originalKeyword":"食蚊鱼"},{"id":"890e12ac-fd37-46d0-885d-41275f574fd8","keyword":"长期暴露","originalKeyword":"长期暴露"},{"id":"4da0db95-5149-4bf0-be3b-b71dbd7be250","keyword":"生物转化酶","originalKeyword":"生物转化酶"}],"language":"zh","publisherId":"hjhx201503006","title":"雄烯二酮长期暴露对食蚊鱼肝脏生物转化酶系的影响?","volume":"","year":"2015"},{"abstractinfo":"采用XRD、XPS和EPMA对中原油田文23-1、23-8气井油管腐蚀产物和管材进行分析,并试验了碳钢在CO_2介质中的腐蚀。研究结果表明,天然气中的CO_2及凝析水是气井腐蚀的主要原因。管材的非金属夹杂物(MnS、Al_2O_3)含量超标,是加速油管在CO_2环境中局部腐蚀穿孔破坏的另一原因。还探索了应用缓蚀剂防止气井CO_2腐蚀的可能性。","authors":[{"authorName":"郑家燊","id":"4aa259a3-9890-4b94-9b92-98f14b4e4f42","originalAuthorName":"郑家燊"},{"authorName":"傅朝阳","id":"a1cacedc-6258-4398-b16d-88cd84d16bb2","originalAuthorName":"傅朝阳"},{"authorName":"刘小武","id":"bf9d6195-ac31-4120-af98-9fe37c032278","originalAuthorName":"刘小武"},{"authorName":"彭芳明","id":"b12594db-16cd-4fed-acee-6a3b80c2e3e0","originalAuthorName":"彭芳明"},{"authorName":"黄先球","id":"81f57758-cf1b-4278-85f5-8487745c85f5","originalAuthorName":"黄先球"},{"authorName":"赵景茂","id":"2585fd88-4683-4422-a42d-a7e16622f802","originalAuthorName":"赵景茂"},{"authorName":"吴灿奇","id":"f5df895d-4271-4238-9ffd-b90f59bcfea3","originalAuthorName":"吴灿奇"},{"authorName":"徐卫东","id":"d818fdc7-f940-4272-876f-da920464a5be","originalAuthorName":"徐卫东"},{"authorName":"王选奎","id":"0e7fcc50-e2ce-4b16-b99e-966d1599adb8","originalAuthorName":"王选奎"}],"categoryName":"|","doi":"","fpage":"227","id":"0d85a2b4-88c6-4d26-9da8-44ae165c2bb0","issue":"3","journal":{"abbrevTitle":"ZGFSYFHXB","coverImgSrc":"journal/img/cover/中国腐蚀封面19-3期-01.jpg","id":"81","issnPpub":"1005-4537","publisherId":"ZGFSYFHXB","title":"中国腐蚀与防护学报"},"keywords":[{"id":"e9abd684-3d59-4d32-afed-0dc9a6ebb526","keyword":"气井","originalKeyword":"气井"},{"id":"419b9942-a4fd-4ee8-a6d7-8dc4eefbc226","keyword":" Oil pipe corrosion","originalKeyword":" Oil pipe corrosion"},{"id":"feeaf218-889a-414d-b05a-0280637a071b","keyword":" Failure analysis","originalKeyword":" Failure analysis"},{"id":"fa46cf1b-a087-49db-976c-f2d91ed2912a","keyword":" Inhibitor","originalKeyword":" Inhibitor"}],"language":"zh","publisherId":"1005-4537_1998_3_5","title":"中原油田文23气田气井腐蚀原因分析","volume":"18","year":"1998"},{"abstractinfo":"以文拉法辛为原料,分别以新的脱甲基试剂半胱氨酸钠盐和青霉胺钠盐制备了O-去甲基文拉法辛,收率为86％和82％.一锅中分别完成了半胱氨酸钠盐、青霉胺钠盐的制备与文拉法辛脱甲基反应,简化了操作步骤.最优反应条件为溶剂N-甲基吡咯烷酮,反应温度175℃,产物析晶pH值9.5.","authors":[{"authorName":"史兰香","id":"7597e205-02a8-4085-8343-0c2ab51f36d3","originalAuthorName":"史兰香"},{"authorName":"张宝华","id":"7ba9bf25-7bfc-4318-8efb-de8c0b997697","originalAuthorName":"张宝华"}],"doi":"10.3724/SP.J.1095.2013.20351","fpage":"608","id":"1c34983e-fdfa-4f09-8d73-f19f35b652d1","issue":"5","journal":{"abbrevTitle":"YYHX","coverImgSrc":"journal/img/cover/YYHX.jpg","id":"73","issnPpub":"1000-0518","publisherId":"YYHX","title":"应用化学"},"keywords":[{"id":"e00801ae-0af6-4f60-8558-f9affd1bf34b","keyword":"O-去甲基文拉法辛","originalKeyword":"O-去甲基文拉法辛"},{"id":"8ca7db3f-40ec-418b-8cdf-abfa3eb3f31f","keyword":"文拉法辛","originalKeyword":"文拉法辛"},{"id":"68c5308b-5920-423a-8b00-745e3794cf01","keyword":"脱甲基化","originalKeyword":"脱甲基化"},{"id":"9a3870aa-9adf-42e1-ba5c-d1ec47baacb2","keyword":"半胱氨酸钠盐","originalKeyword":"半胱氨酸钠盐"},{"id":"cc5917c0-e45e-49e1-ba0f-753dc1f71b26","keyword":"青霉胺钠盐","originalKeyword":"青霉胺钠盐"}],"language":"zh","publisherId":"yyhx201305020","title":"O-去甲基文拉法辛合成的新方法","volume":"30","year":"2013"},{"abstractinfo":"对丽文哈贝壳的微结构进行了扫描电镜(SEM)观察,观察显示它是由无机霰石层和有机胶原蛋白组成的一种生物陶瓷复合材料,其中无机霰石层平行于贝壳表面整齐排列.观察也显示这些霰石层是由长而薄的霰石片所组成,不同霰石层中的霰石片具有不同的方向,构成螺旋等铺层形式.更仔细的观察显示每一霰石片又是由长而细的霰石纤维所组成,最细的霰石纤维具有纳米的尺度.根据在贝壳中观察到的螺旋结构,进行了螺旋结构和平行结构最大拔出力的比较实验研究,结果显示螺旋结构的最大拔出力大于平行结构的最大拔出力,它使贝壳具有高的强韧性.研究结果对高性能仿生陶瓷复合材料设计提供了有益指导.","authors":[{"authorName":"陈斌","id":"91984828-0e77-4a93-8cfd-2a46e2d25fed","originalAuthorName":"陈斌"},{"authorName":"彭向和","id":"d5ef20d1-e4e5-4a98-ba6b-92196ea2e073","originalAuthorName":"彭向和"},{"authorName":"孙士涛","id":"75180f74-ebf9-43d4-8789-47a26820e62b","originalAuthorName":"孙士涛"},{"authorName":"季金苟","id":"40f27576-f5ed-4e6e-b90d-d14547d07392","originalAuthorName":"季金苟"},{"authorName":"陈松","id":"964db22e-7bbb-4c54-80ae-5085d2652f09","originalAuthorName":"陈松"}],"doi":"","fpage":"60","id":"3b75f394-59d0-43b2-a932-20048ca15d0a","issue":"z1","journal":{"abbrevTitle":"XYJSCLYGC","coverImgSrc":"journal/img/cover/XYJSCLYGC.jpg","id":"69","issnPpub":"1002-185X","publisherId":"XYJSCLYGC","title":"稀有金属材料与工程"},"keywords":[{"id":"27c2d5d0-a910-4ad5-877a-f290d9c33e02","keyword":"丽文哈贝壳","originalKeyword":"丽文哈贝壳"},{"id":"9b386643-5818-48f6-b972-95cb3df8690a","keyword":"生物陶瓷复合材料","originalKeyword":"生物陶瓷复合材料"},{"id":"1282b5cd-aa58-48ae-816f-8792bfb44248","keyword":"螺旋微结构","originalKeyword":"螺旋微结构"},{"id":"aadcdba1-cd86-4a6e-839e-1b9c5dec2ce3","keyword":"最大拔出力","originalKeyword":"最大拔出力"}],"language":"zh","publisherId":"xyjsclygc2008z1015","title":"丽文哈贝壳螺旋微结构研究","volume":"37","year":"2008"}],"totalpage":16,"totalrecord":158}