以二甲基亚砜(DMSO)为溶剂进行溶液聚合制得聚丙烯腈(PAN)溶液,在此溶液中混入了微米级铁粉后将其压成薄膜,将烘干后的薄膜高温碳化处理制得一种碳基吸波材料。采用X射线衍射(XRD)、扫描电镜(SEM)等手段对材料的成分、形貌、结构进行了表征。采用矢量网络分析仪对该复合材料在2~18GHz频段内的电磁参数进行了测试,并作了微波反射率的数值模拟。研究了碳化温度对材料物相组成和电磁性能的影响以及碳化温度和涂层厚度对材料吸波性能的影响。此种吸波材料是无定形炭和铁的氧化物、铁的氮化物等磁性物质的复合材料,兼有电损耗和磁损耗,具有较好的吸波性能。
Electromagnetic wave absorption material comprised of amorphous carbon and magnetic particles was prepared by heat treatment of polyacrylonitrile(PAN) with ultrafine iron powders dispersed in it.The phase composition and morphology of the material were characterized by X-ray diffraction(XRD) and scanning electron microscopy(SEM),respectively.Electromagnetic parameters of the composite material were measured in the frequency range of 2-18 GHz by vector network analyzer and the numerical simulation of microwave reflection loss was conducted.The effects of temperature and coating thickness on electromagnetic wave absorption properties were investigated.This kind of absorbing material is a composite material comprised of amorphous carbon and iron oxide,or iron nitride with electric loss and magnetic loss,and has good absorbing properties.
参考文献
[1] | 邢丽英.隐身材料[M].北京:化学工业出版社,2004 |
[2] | 王晨,顾家琳,康飞宇.吸波材料理论设计的研究进展[J].材料导报,2009(05):5-8. |
[3] | Bi Cheng;Zhu Meifang;Zhang Qinghong et al.Electromagnetic wave absorption properties of multi-walled car bon nanotubes decorated with La-doped BaTiO3 nanocrystals synthesized by a solvothermal method[J].Materials Chemistry and Physics,2011,126:596-601. |
[4] | 王祖鹏,于名讯,潘士兵,厉宁,刘永峙.纤维复合吸波材料的研究进展[J].化工新型材料,2010(04):13-15. |
[5] | 吴红焕,王晓艳,张玲,朱冬梅,周万城.碳纤维吸波材料的研究进展[J].材料导报,2007(05):115-117,124. |
[6] | 罗发,周万城,焦桓,赵东林.高温吸波材料研究现状[J].宇航材料工艺,2002(01):8-11. |
[7] | X-Band microwave characterization of carbon-based nanocomposite material, absorption capability comparison and RAS design simulation[J].Composites science and technology,2010(2):400. |
[8] | Liu X G;Ou Z Q;Geng D Y .Enhanced absorption bandwidth in carbon-coated supermalloy FeNiMo nanocapsules for a thin absorb thickness[J].Journal of Alloys and Compounds,2010,506:826-830. |
[9] | 安玉良,王俊,袁霞,刘艳秋.碳包覆铁纳米颗粒制备及电磁性能分析[J].纳米技术与精密工程,2010(01):16-19. |
- 下载量()
- 访问量()
- 您的评分:
-
10%
-
20%
-
30%
-
40%
-
50%