双胺类发光材料的合成及光电化学性能研究

合成材料老化与应用, 2016, 45(5): 51-61.

双胺类发光材料的合成及光电化学性能研究

蒋卫鹏 ^1, , 李继 ^2, , 王文新 ^3, , 陈海涛 ^4,

1.河南省科学院化学研究所有限公司,河南郑州,450002

2.河南省科学院化学研究所有限公司,河南郑州,450002

3.河南省科学院化学研究所有限公司,河南郑州,450002

4.河南省科学院化学研究所有限公司,河南郑州,450002

关键词： 2,7-二溴咔唑 , 热稳定性 , 光学性能 , 电化学性能

Synthesis and Photoelectrochemical Performance Study of Diamante Luminescent Materials

Keywords： 2,7-dibromocarbazole , thermal stability , optical performance , electrochemical performance

以2,7-二溴咔唑为起始原料,经Ullmann、Buchwald-Hartwig偶联反应合成了目标化合物,通过NMR、IR和MS表征了化合物的结构,经DSC-TG、UV、荧光光谱分析和循环伏安法研究了目标化合物的热稳定性、光学及电化学性能.

The target compound was synthesized by Ullmann reaction,Buchwald-Hartwig coupling reaction using 2,7-dibromocarbazole as starting materials. The structure of the target compound was characterized by NMR,IR and MS. Thermal properties,optical properties and electrochemical performance were determined with DSC-TG,UV,CV and the fluorescence spectrum analysis.

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