利用电子束快退火法制备了MgB2超导薄膜.该方法利用高能电子束,在中真空条件下照射Mg-B多层前驱膜,照射时间维持在1s以下.在电子束的作用下,前驱膜中的Mg和B迅速反应,形成MgB2相.整个退火过程没有Mg蒸气与氩气保护,极短的退火时间有效地限制了前驱膜中Mg的流失和Mg与其它物质的反应.与传统制备工艺相比,该方法避免了混合物理化学气相沉积法中乙硼烷的使用;省去异位退火法中提供高Mg蒸气压的限制,避免在有Mg块存在情况下退火后样品表面存在Mg污染的问题.利用该方法在SiC(001)衬底上生长了100nm厚的MgB2薄膜,其超导转变温度Tc~35K,均方根粗糙度为3.6nm,临界电流密度Jc(5K,0 T) =3.8×106 A/cm2.该方法对MgB2薄膜的大规模工业生产提供了一个新思路.
参考文献
[1] | Nagamatsu J;Nakagawa N;Muranaka T;Zenitani Y;Akimitsu J .Superconductivity at 39 K in magnesium diboride[J].Nature,2001(6824):63-64. |
[2] | Finnemore DK.;Bud'ko SL.;Lapertot G.;Canfield PC.;Ostenson JE. .Thermodynamic and transport properties of superconducting (MgB2)-B-10[J].Physical review letters,2001(11):2420-2422. |
[3] | Kleinsasser A.W. .High performance Nb Josephson devices for petaflops computing[J].IEEE Transactions on Applied Superconductivity: A Publication of the IEEE Superconductivity Committee,2001(1):1043-1049. |
[4] | Wu YS;Zhao Y;Wexler D;Kim JH;Dou SX .Optimization of in situ annealing conditions for off-axis PLD MgB2 films[J].Physica, C. Superconductivity and its applications,2008(3):218-222. |
[5] | Xi X.X.;Zeng X.H.;Pogrebnyakov A.V.;Xu S.Y.;Qi Li;Yu Zhong;Brubaker C.O.;Zi-Kui Liu;Lysczek E.M.;Redwing J.M.;Lettieri J.;Schlom D.G.;Tian W.;Pan X.Q. .In situ growth of MgB<SUB>2</SUB> thin films by hybrid physical-chemical vapor deposition[J].IEEE Transactions on Applied Superconductivity: A Publication of the IEEE Superconductivity Committee,2003(2):3233-3237. |
[6] | Dai, Q.;Kong, X.;Feng, Q.;Yang, Q.;Zhang, H.;Nie, R.;Han, L.;Ma, Y.;Wang, F..MgB _2 films prepared by rapid annealing method[J].Physica, C. Superconductivity and its applications,2012:24-27. |
[7] | Jo W.;Beasley M.R.;Hammond R.H. .Anisotropy and critical current density of MgB<SUB>2</SUB> thin films grown in-situ by molecular beam epitaxy[J].IEEE Transactions on Applied Superconductivity: A Publication of the IEEE Superconductivity Committee,2003(2):3257-3260. |
上一张
下一张
上一张
下一张
计量
- 下载量()
- 访问量()
文章评分
- 您的评分:
-
10%
-
20%
-
30%
-
40%
-
50%