对2507超级双相不锈钢在920℃进行了不同保温时间的时效处理,采用光学显微镜、扫描电镜、X射线衍射仪和能谱仪分析了不同时效状态下的组织演变规律,通过硬度试验和冲击试验研究了时效时间对2507超级双相不锈钢性能的影响.结果表明,920℃时效处理时,大量的σ相沿γ/α及α/α晶界析出,并向铁素体内部长大,其形成机理为铁素体共析转变成σ相和二次奥氏体γ2;在时效5 min内σ相的析出速率最快,随着时效时间的延长,σ相的含量增加,但析出速率逐渐变小;σ相的出现严重降低了超级双相不锈钢的冲击韧性,并且使其硬度明显增加,冲击功和硬度值的大小与σ相析出量有关,当920℃时效30 min时,σ析出相的含量接近于28%,对应双相不锈钢的冲击功和硬度值分别为6 J和376 HB.
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