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采用机械合金化与热压烧结工艺制备了添加合金元素Ⅴ和Fe的Laves相增强的Nb基复合材料.研究了添加质量分数4%Ⅴ和Fe的Nb/NbCr2-4.0V和Nb/NbCr2-4.0Fe配比成分的元素粉,经MA 20 h后在1250℃热压30 min所获得的Nb/NbCr2合金的组织和性能.结果表明:在热压过程中原位合成出细小弥散分布的三元Laves相Nb(Cr,Ⅴ)2和Nb(Cr,Fe)2,并且V和Fe原子只占据Laves相中的Cr原子位置.制备出的Laves相增强Nb基合金接近全致密,组织细小均匀,晶粒尺寸小于500 nm.Nb/NbCr2-4.0V和Nb/NbCr2-4.0Fe合金的断裂韧性分别达到5.3和6.3 MPa·m1/2,其中Nb/NbCr2-4.0Fe合金不仅抗压强度达到2256 MPa,其屈服强度和塑性应变也分别达到2094MPa和6.03%.

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