本实验通过等温退火(200℃)等径角挤压(Equal Channel Angular Pressing,ECAP)制备的超细晶铜获得了双模晶粒分布(Bimodal)的铜样品.力学性能测试显示该双模晶粒分布铜样品具有很好的强度和塑性的综合性能(屈服强度225MPa,断裂延伸率20%).进而利用电子背散射衍射(EBSD)技术研究了同一微观区域在拉伸应变分别为0%、3%、8%、14%时的微观结构信息,发现在拉伸过程中,部分超细晶晶粒和再结晶粗晶晶粒均发生了转动,粗晶晶粒内部出现了较大的局部应变以及亚晶界.此外,拉伸过程中伴随着部分退火孪晶的消失和小角晶界的增多,导致拉伸后平均晶粒尺寸下降.
参考文献
[1] | R.Z.Valiev;I.V.Alexandrov;Y.T.Zhu .Paradox for strength and ductility in metals processed by severe plastic deformation[J].Journal of Materials Research,2002(1):5-8. |
[2] | Legros M.;Rittner MN.;Weertman JR.;Hemker KJ.;Elliott BR. .Microsample tensile testing of nanocrystalline metals[J].Philosophical Magazine.A.Physics of condensed matter, defects and mechanical properties,2000(4):1017-1026. |
[3] | C. C. Koch;D. G. Morris;K. Lu .Ductility of Nanostructured Materials[J].MRS bulletin,1999(2):54-58. |
[4] | J. R. Weertman;D. Farkas;K. Hemker .Structure and Mechanical Behavior of bulk Nanocrystalline Materials[J].MRS bulletin,1999(2):44-50. |
[5] | 邬震泰,屠曹富.高温高压旋转接头伺服环构件用纳米结构铜合金[J].材料科学与工程学报,2012(06):849-852. |
[6] | 陈劲松,赵阳培,杨建明,乔斌.纳米晶铜电火花电极快速制造及其耐电蚀性能[J].材料科学与工程学报,2012(02):188-191,196. |
[7] | Wang Y;Chen M;Zhou F;Ma E .High tensile ductility in a nanostructured metal.[J].Nature,2002(6910):912-915. |
[8] | V.L. TELLKAMP;A. MELMED;E.J. LAVERNIA .Mechanical Behavior and Microstructure of a Thermally Stable Bulk Nanostructured Al Alloy[J].Metallurgical and Materials Transactions, A. Physical Metallurgy and Materials Science,2001(9):2335-2343. |
[9] | Yonghao Zhao;Troy Topping;Ying Li;Enrique J. Lavernia .Strength and Ductility of Bi-Modal Cu[J].Advanced Engineering Materials,2011(9):865-871. |
[10] | Y.S. Li;Y. Zhang;N.R. Tao .Effect of thermal annealing on mechanical properties of a nanostructured copper prepared by means of dynamic plastic deformation[J].Scripta materialia,2008(4):475-478. |
[11] | ZONGHOON LEE;VELIMIR RADMILOVIC;BYUNGMIN AHN .Tensile Deformation and Fracture Mechanism of Bulk Bimodal Ultrafine-Grained Al-Mg Alloy[J].Metallurgical and Materials Transactions, A. Physical Metallurgy and Materials Science,2010(4):795-801. |
[12] | A.V. Sergueeva;N.A. Mara;R.Z. Valiev .Elevated temperature behavior of SePD materials: Superplasticity or enhanced ductility?[J].Materials Science & Engineering, A. Structural Materials: Properties, Misrostructure and Processing,2005(0):413-416. |
[13] | Budrovic Z;Van Swygenhoven H;Derlet PM;Van Petegem S;Schmitt B .Plastic deformation with reversible peak broadening in nanocrystalline nickel[J].Science,2004(5668):273-276. |
[14] | G E Dieter.Mechanical Metallurgy[M].McGraw-Hill Book Co.,New York,1988:289-290. |
[15] | M.A. Meyers;A. Mishra;D.J. Benson .Mechanical properties of nanocrystalline materials[J].Progress in materials science,2006(4):427-556. |
[16] | Fan GJ;Choo H;Liaw PK;Lavernia EJ .Plastic deformation and fracture of ultrafine-grained Al-Mg alloys with a bimodal grain size distribution[J].Acta materialia,2006(7):1759-1766. |
[17] | 束德林.工程材料力学性能[M].安徽合肥:机械工业出版社:6-7. |
[18] | Chen, P.;Mao, S.C.;Liu, Y.;Wang, F.;Zhang, Y.F.;Zhang, Z.;Han, X.D..In-situ EBSD study of the active slip systems and lattice rotation behavior of surface grains in aluminum alloy during tensile deformation[J].Materials Science & Engineering, A. Structural Materials: Properties, Misrostructure and Processing,2013:114-124. |
[19] | Shigeaki Kobayashi;Tatsuya Maruyama;Sakae Saito;Sadahiro Tsurekawa;Tadao Watanabe .In situ observations of crack propagation and role of grain boundary microstructure in nickel embrittled by sulfur[J].Journal of Materials Science,2014(11):4007-4017. |
[20] | Z Lee;J Lee;E J.Lavernia;S R Nutt.Experiment and FEM analysis of tensile behavior of bimodal nanocrystalline Al-Mg alloys[A].,2004(821):257-262. |
上一张
下一张
上一张
下一张
计量
- 下载量()
- 访问量()
文章评分
- 您的评分:
-
10%
-
20%
-
30%
-
40%
-
50%