欢迎登录材料期刊网

材料期刊网

高级检索

研究了颗粒级配对超细氧化铝粉体成型行为和烧结行为的影响.发现两种颗粒直径之比约为2的氧化铝粉体,一定比例混合后可获得比同样条件下单独的粉体高得多的成型密度.在细颗粒体积百分数约为33%时,应用压滤成型工艺(45MPa)获得的素坯相对密度高达72%.研究了压滤和干压成型方法对成型素坯密度及其烧结的影响.压滤成型的素坯,由于成型密度高、气孔分布窄、孔径小而有利于烧结,在较低的温度下可以达到理论密度,烧结体晶粒细小均匀,无明显缺陷;这一条件下于压成型(300MPa)得到的素坯由于有较宽的气孔尺寸分布,影响烧结,并且烧结体中有较大的气孔,不能完全致密.应用新的烧结理论对此进行了解释.

The effcct of bimodal partiele size distribution on the compact cfficiency and sintering behavior ofsubmicron-sized alumina powder was investigated For two types of submicroll alumina powders with sizeratio of about 2, collsidcrably lligller compact densitics, as compared to their individuaJs, were obtainedwhen mixed in proper volumc ratios. In the casc of 33% fine particls in the mixed powder, the relativegreen density of abovc 72% was achieved by pressure filtration. Different consolidation techniqucs, namely pressure filtration and drying press, were found to yield compacts with different properties. Green compacts by pressure filtration, which had higher density, narrower pore size distribution and smaller mean pore size than those by dry-pressing, can be sintered to theoretical density with fine microstructure at relatively low temperature. The sintering behavior and the microstructure developed for the compacts by different compaction techniques were discussed with newly developed theory of sintering thermodynamics.

参考文献

[1]
上一张 下一张
上一张 下一张
计量
  • 下载量()
  • 访问量()
文章评分
  • 您的评分:
  • 1
    0%
  • 2
    0%
  • 3
    0%
  • 4
    0%
  • 5
    0%