采用反应热压烧结法制备了SiC/Ti3SiC2复合材料,研究了热压温度、SiC含量及粒度对SiC/Ti3SiC2复合材料相组成、力学性能以及应力-应变行为的影响.结果表明:热压温度影响SiC/Ti3SiC2复合材料相组成;随着热压温度的提高,复合材料的弯曲强度和断裂韧性提高;随SiC含量的增加,SiC/Ti3SiC2复合材料弯曲强度和断裂韧性提高,当SiC的质量分数为30%时,弯曲强度为371 MPa,断裂韧性为6.9 MPa·m1/2;但SiC的质量分数达到50%时,由于复合材料含有较多的孔洞,使强度和断裂韧性降低;随着SiC粒度的增大,复合材料易于致密化,使其弯曲强度和断裂韧性提高;SiC/Ti3SiC2复合材料在常温下表现为非脆性断裂.
参考文献
[1] | Luo Y M,Zheng Z M,Mei X N,Xu C H.Growth mechanism of Ti3 SiC2 single crystals by in situ reaction of polycarbosilane and metal titanium with CaF2 additive[J].Journal of Crystal Growth,2008,310(14):3372-3375. |
[2] | Zhang Y,Zhou Y C,Li Y Y.Solid-liquid synthesis of Ti3SiC2particulate by fluctuation procedure[J].Scripta Materialia,2003,49:249-253. |
[3] | Yeh C L,Shen Y G,Effects of SiC addition on formation of Ti3 SiC2 by self-propagating high-temperature synthesis[J].Journal of Alloys and Compounds,2008,461:654-660. |
[4] | Lin T C,Hon M H.Synthesis and microstructure of the Ti3 SiC2 in SiC matrix grown by chemical vapor deposition[J].Ceramics International,2008,34:63 1-638. |
[5] | Zou Y,Sun Z M.Tada Shuji,Hitoshi Hashimoto.Synthesis reactions for Ti3SiC2 through pulse discharge sintering TiH2/Si/TiC powder mixture[J].Materials Research Bulletin,2008,43:968-975. |
[6] | Zhang Z F,Sun Z M.Shear fracture behavior of Ti3SiC2 induced by compression at temperatures below 1000 ℃[J].Materials Science and Engineering A,2005,408:64-71. |
[7] | Radovic M,Barsoum M W,El-Raghy T,Wiederhorn S M,Luecke W E.Effect of temperature,strain rate and grain size on the mechanical response of Ti3SiC2 in tension[J].Acta Materialia,2002,50:1297-1306. |
[8] | 李世波,成来飞,王东,张立同.层状Ti3SiC2陶瓷的组织结构及力学性能[J].复合材料学报,2002,19(6):20-24.Li Shibo,Cheng Laifei,Wang Dong,Zhang Litong.Microstructure and mechanical properties of Ti3SiC2 ceramics[J].Acta Materiae Compositae Sinica,2002,19(6):20-24. |
[9] | Li S B,Xie J X,Zhang L T,Cheng L F,Mechanical properties and oxidation resistance of Ti3SiC2/SiC composite synthesized by in situ displacement reaction of Si and TiC[J].Materials Letters,2003,57:3048-3056. |
[10] | Zhang J F,Wang L J,Jiang W,Chen L D.High temperature oxidation behavior and mechanism of Ti3 SiC2-SiC nanocomposites in air[J].Composites Science and Technology,2008,68:1531-1538. |
[11] | 尹洪峰,范强,任耘,张军战.SiC含量对Ti3SiC2/SiC复合材料性能的影响[J].航空材料学报,2008,28(6):78-81.Yin Hongfeng,Fan Qiang,Ren Yun,Zhang Junzhan.Effect of content of SiC on properties of Ti3 SiC2/SiC composites[J].Journal of Aeronautical Materials,2008,28(6):78-81. |
[12] | Yang S L,Sun Z M,Hitoshi Hashimoto.Reaction in Ti3 SiC2 powder synthesis from a Ti-Si-TiC powder mixture[J].Journal of Alloys and Compounds,2004,368:312-317. |
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